(Ni(Me₂⁽¹⁴⁾dienatoN₂P₂))PF₆

Base Information

Chemical Name:(Ni(Me₂⁽¹⁴⁾dienatoN₂P₂))PF₆
CAS No.:80161-01-9
Molecular Formula:C₂₄H₃₁N₂NiP₂*F₆P
Molecular Weight:613.125
Hs Code.:

(Ni(Me<sub>2</sub><sup>(14)</sup>dienatoN<sub>2</sub>P<sub>2</sub>))PF<sub>6</sub>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Ni(Me₂⁽¹⁴⁾dienatoN₂P₂))PF₆

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Technology Process of (Ni(Me₂⁽¹⁴⁾dienatoN₂P₂))PF₆

There total 1 articles about (Ni(Me₂⁽¹⁴⁾dienatoN₂P₂))PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: sodium hexaflorophosphate

: 6018-89-9
nickel(II) acetate tetrahydrate

: 80160-69-6
1,3-bis[(2-aminoethyl)phenylphosphino]propane

: 80161-01-9
(Ni(Me₂⁽¹⁴⁾dienatoN₂P₂))PF₆

Guidance literature:: With acetylacetone; acetic acid; In methanol; water; acetylacetone in MeOH added dropwise to soln. 2,3,2-N2P2 in methanol, soln. refluxed for 16 h, soln. Ni(OAc)2*4H2O in MeOH added dropwise, soln. refluxed for 16 h, 90% MeOH removed, H2O containing acetic acid added (pH 4), aq. soln. NaPF6 added; ppt. purified by column chromy. with basic alumina as support and 95% EtOH as eluant; elem. anal.;
DOI:10.1021/ic00133a067