C₃₀H₃₁NO₄

Base Information

Chemical Name:C₃₀H₃₁NO₄
CAS No.:1372812-52-6
Molecular Formula:C₃₀H₃₁NO₄
Molecular Weight:469.58
Hs Code.:

C<sub>30</sub>H<sub>31</sub>NO<sub>4</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₀H₃₁NO₄

Chemical Property:

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Technology Process of C₃₀H₃₁NO₄

There total 7 articles about C₃₀H₃₁NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1372812-51-5
C₃₃H₃₉NO₄Si

: 1372812-52-6
C₃₀H₃₁NO₄

Guidance literature:: With cesium fluoride; In tetrahydrofuran; methanol; at 20 ℃; for 1h;
DOI:10.1039/c2jm16847b

Reference yield:

: 586-76-5
4-Bromobenzoic acid

: 1372812-52-6
C₃₀H₃₁NO₄

Guidance literature:: Multi-step reaction with 6 steps

1: thionyl chloride; N,N-dimethyl-formamide / 1 h / Reflux

2: tetrahydrofuran / 1 h / 0 - 5 °C

3: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri-tert-butylphosphonium tetrafluoroborate; potassium tert-butylate / toluene / 2 h / 20 °C

4: zinc diacetate; Iodine monochloride / 1,4-dioxane / 3 h / 20 °C

5: piperidine; copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride / 60 °C

6: cesium fluoride / tetrahydrofuran; methanol / 1 h / 20 °C

With piperidine; bis-triphenylphosphine-palladium(II) chloride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; copper(l) iodide; thionyl chloride; tri-tert-butylphosphonium tetrafluoroborate; potassium tert-butylate; zinc diacetate; Iodine monochloride; N,N-dimethyl-formamide; cesium fluoride; In tetrahydrofuran; 1,4-dioxane; methanol; toluene; 5: Sonogashira coupling;
DOI:10.1039/c2jm16847b

Reference yield:

: 59247-47-1
tert-butyl-4-bromobenzoate

: 1372812-52-6
C₃₀H₃₁NO₄

Guidance literature:: Multi-step reaction with 4 steps

1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri-tert-butylphosphonium tetrafluoroborate; potassium tert-butylate / toluene / 2 h / 20 °C

2: zinc diacetate; Iodine monochloride / 1,4-dioxane / 3 h / 20 °C

3: piperidine; copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride / 60 °C

4: cesium fluoride / tetrahydrofuran; methanol / 1 h / 20 °C

With piperidine; bis-triphenylphosphine-palladium(II) chloride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; copper(l) iodide; tri-tert-butylphosphonium tetrafluoroborate; potassium tert-butylate; zinc diacetate; Iodine monochloride; cesium fluoride; In tetrahydrofuran; 1,4-dioxane; methanol; toluene; 3: Sonogashira coupling;
DOI:10.1039/c2jm16847b