Technology Process of C36H43N3O5
There total 17 articles about C36H43N3O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triethylamine;
In
dichloromethane;
at 0 ℃;
for 1h;
DOI:10.1021/jm400542h
- Guidance literature:
-
Multi-step reaction with 12 steps
1: hydrogenchloride / methanol; ethyl acetate / 5 h / 20 °C
2: sodium carbonate / tetrahydrofuran; water / 12 h / 20 °C
3: Dess-Martin periodane / dichloromethane / 0.5 h / 20 °C
4: 2-methyl-but-2-ene; sodium dihydrogenphosphate dihydrate; sodium chlorite / tetrahydrofuran; tert-butyl alcohol; water / 14 h / 20 °C
5: triethylamine; diphenyl phosphoryl azide / dichloromethane / 17.33 h / 0 - 20 °C
6: 29 h / Reflux
7: potassium carbonate / methanol / 14 h / 20 °C
8: triethylamine / dichloromethane / 3 h / 0 - 20 °C
9: trifluoroacetic acid / dichloromethane / 1 h / 20 °C
10: triethylamine / dichloromethane / 19 h / 0 - 20 °C
11: trifluoroacetic acid; palladium on activated charcoal; hydrogen / tetrahydrofuran / 1 h / 0 °C
12: triethylamine / dichloromethane / 1 h / 0 °C
With
hydrogenchloride; sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; diphenyl phosphoryl azide; palladium on activated charcoal; hydrogen; sodium carbonate; potassium carbonate; Dess-Martin periodane; triethylamine; trifluoroacetic acid;
In
tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; tert-butyl alcohol;
3: |Dess-Martin Oxidation;
DOI:10.1021/jm400542h
- Guidance literature:
-
Multi-step reaction with 4 steps
1: triethylamine / dichloromethane / 1 h / 0 °C
2: triethylamine / dichloromethane / 19 h / 0 - 20 °C
3: trifluoroacetic acid; palladium on activated charcoal; hydrogen / tetrahydrofuran / 1 h / 0 °C
4: triethylamine / dichloromethane / 1 h / 0 °C
With
palladium on activated charcoal; hydrogen; triethylamine; trifluoroacetic acid;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/jm400542h