[(η6-p-cymene)RuCl2(1-(4-cyanophenyl)imidazole)]

Base Information

Chemical Name:[(η6-p-cymene)RuCl2(1-(4-cyanophenyl)imidazole)]
CAS No.:832103-24-9
Molecular Formula:C₂₀H₂₁Cl₂N₃Ru
Molecular Weight:475.383
Hs Code.:

Synonyms:

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Chemical Property of [(η6-p-cymene)RuCl2(1-(4-cyanophenyl)imidazole)]

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Technology Process of [(η6-p-cymene)RuCl2(1-(4-cyanophenyl)imidazole)]

There total 1 articles about [(η6-p-cymene)RuCl2(1-(4-cyanophenyl)imidazole)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 52462-29-0
[ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂

: 25372-03-6
4-(1H-imidazol-1-yl)benzonitrile

: 832103-24-9
[(η6-p-cymene)RuCl2(1-(4-cyanophenyl)imidazole)]

Guidance literature:: In dichloromethane; N2 atm.; a suspn. of complex in CH2Cl2 was treated with imidazole-compound, stirred at room temp. for 4 h; evapd. to dryness under reduced pressure, extd. with CH2Cl2, filtered, light petroleum was added with stirring, crystals were filtered, washed with petroleum ether, dried under vac.; elem. anal.;
DOI:10.1021/ic049256m

Reference yield: 75.0%

: ammonium hexafluorophosphate

: 66-71-7
1,10-Phenanthroline

: 832103-24-9
[(η6-p-cymene)RuCl2(1-(4-cyanophenyl)imidazole)]

: [(η6-p-cymene)Ru(1,10-phenanthroline)(1-(4-cyanophenyl)imidazole)](PF6)2

Guidance literature:: In methanol; N2 atm.; a suspn. of complex and phenanthroline in methanol was heated under reflux for 1 h, cooled to room temp., filtered, NH4PF6 in methanol was added; solid was filtered out, washed with methanol and diethyl ether; elem. anal.;
DOI:10.1021/ic049256m

Reference yield: 73.0%

: 13826-83-0
ammonium tetrafluroborate

: 832103-24-9
[(η6-p-cymene)RuCl2(1-(4-cyanophenyl)imidazole)]

: 603-35-0
triphenylphosphine

: 832103-29-4
[(η6-p-cymene)RuCl(1-(4-cyanophenyl)imidazole)PPh3]BF4

Guidance literature:: In methanol; N2 atm.; PPh3 was added to a suspn. of complex in methanol, heated underreflux for 1 h, cooled to room temp., filtered, NH4BF4 in methanol was added; solid was filtered out, washed with methanol and diethyl ether; elem. anal.;
DOI:10.1021/ic049256m