(phenylimido)vanadium(V) triisopropoxide dimer

Base Information

Chemical Name:(phenylimido)vanadium(V) triisopropoxide dimer
CAS No.:1051365-40-2
Molecular Formula:C₃₀H₅₂N₂O₆V₂
Molecular Weight:638.636
Hs Code.:

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Chemical Property of (phenylimido)vanadium(V) triisopropoxide dimer

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Technology Process of (phenylimido)vanadium(V) triisopropoxide dimer

There total 1 articles about (phenylimido)vanadium(V) triisopropoxide dimer which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 5588-84-1
vanadium(V) oxytriisopropoxide

: 103-71-9
phenyl isocyanate

: 1051365-40-2
(phenylimido)vanadium(V) triisopropoxide dimer

Guidance literature:: In neat (no solvent); under N2; mixt. of V compd. and isocyanate stirred at 140°C for 3h; cooled to room temp.; CH2Cl2 added; filtered; filtrate evapd. under reduced pressure; recrystd. from hexane or CH2Cl2 at -30°C;
DOI:10.1021/ic800528m