C₁₅H₂₆O

Base Information

Chemical Name:C₁₅H₂₆O
CAS No.:275825-12-2
Molecular Formula:C₁₅H₂₆O
Molecular Weight:222.371
Hs Code.:

Synonyms:

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Chemical Property of C₁₅H₂₆O

Chemical Property:

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Technology Process of C₁₅H₂₆O

There total 7 articles about C₁₅H₂₆O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (2R)-2-methyl-5-(2-methyl-7-oxabicyclo[4.1.0]heptan-2-yl)pent-1-en-3-yl acetate

: 275825-12-2
C₁₅H₂₆O

Guidance literature:: Multi-step reaction with 4 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; tributylphosphine; ammonium formate / 1,4-dioxane / 3 h / Reflux

2: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Inert atmosphere; Reflux

3: Dess-Martin periodane / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

4: tetrahydrofuran; benzene / 1 h / 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tributylphosphine; ammonium formate; Dess-Martin periodane; In tetrahydrofuran; 1,4-dioxane; dichloromethane; benzene;
DOI:10.1002/anie.201104331

Reference yield:

: 1344731-02-7
(2R)-2-methyl-2-(4-methylpent-4-en-1-yl)-7-oxabicyclo[4.1.0]heptanes

: 275825-12-2
C₁₅H₂₆O

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Inert atmosphere; Reflux

2: Dess-Martin periodane / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

3: tetrahydrofuran; benzene / 1 h / 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; Dess-Martin periodane; In tetrahydrofuran; dichloromethane; benzene;
DOI:10.1002/anie.201104331

Reference yield:

: 1344731-01-6
2-methyl-5-((S)-1-methylcyclohex-2-en-1-yl)pent-1-en-3-yl acetate

: 275825-12-2
C₁₅H₂₆O

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 4 h

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; tributylphosphine; ammonium formate / 1,4-dioxane / 3 h / Reflux

3: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Inert atmosphere; Reflux

4: Dess-Martin periodane / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

5: tetrahydrofuran; benzene / 1 h / 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tributylphosphine; ammonium formate; sodium hydrogencarbonate; Dess-Martin periodane; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; 1,4-dioxane; dichloromethane; benzene;
DOI:10.1002/anie.201104331