C₂₈H₃₀N₄O₅S

Base Information

Chemical Name:C₂₈H₃₀N₄O₅S
CAS No.:745019-79-8
Molecular Formula:C₂₈H₃₀N₄O₅S
Molecular Weight:534.636
Hs Code.:

C<sub>28</sub>H<sub>30</sub>N<sub>4</sub>O<sub>5</sub>S

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₈H₃₀N₄O₅S

Chemical Property:

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Technology Process of C₂₈H₃₀N₄O₅S

There total 10 articles about C₂₈H₃₀N₄O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 745020-01-3
C₃₆H₃₂N₄O₇S

: 745019-79-8
C₂₈H₃₀N₄O₅S

Guidance literature:: With hydrazine hydrate; In ethanol; at 50 ℃;
DOI:10.1016/j.bmcl.2013.06.027

Reference yield:

: 1448959-28-1
C₁₃H₁₇NO₃

: 745019-79-8
C₂₈H₃₀N₄O₅S

Guidance literature:: Multi-step reaction with 9 steps

1.1: hydrogenchloride / 48 h / 0 °C

1.2: 1 h

2.1: water; lithium hydroxide / tetrahydrofuran / 20 °C

3.1: caesium carbonate / N,N-dimethyl-formamide / 20 °C

4.1: triethylamine; methanesulfonyl chloride / dichloromethane / 0 - 20 °C

5.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 17 h / 90 °C

6.1: palladium 10% on activated carbon; hydrogen / tetrahydrofuran / 3102.97 Torr

7.1: triethylamine; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate / N,N-dimethyl-formamide; dichloromethane

8.1: Chiral Pak OD / Resolution of racemate

9.1: hydrazine hydrate / ethanol / 50 °C

With hydrogenchloride; palladium 10% on activated carbon; water; hydrogen; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; caesium carbonate; hydrazine hydrate; methanesulfonyl chloride; triethylamine; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2013.06.027

Reference yield:

: 745019-94-7
C₁₃H₁₈O₅

: 745019-79-8
C₂₈H₃₀N₄O₅S

Guidance literature:: Multi-step reaction with 7 steps

1: caesium carbonate / N,N-dimethyl-formamide / 20 °C

2: triethylamine; methanesulfonyl chloride / dichloromethane / 0 - 20 °C

3: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 17 h / 90 °C

4: palladium 10% on activated carbon; hydrogen / tetrahydrofuran / 3102.97 Torr

5: triethylamine; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate / N,N-dimethyl-formamide; dichloromethane

6: Chiral Pak OD / Resolution of racemate

7: hydrazine hydrate / ethanol / 50 °C

With palladium 10% on activated carbon; hydrogen; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; caesium carbonate; hydrazine hydrate; methanesulfonyl chloride; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2013.06.027