2-Phenylspiro[cyclopropane-1,9'-fluorene]

Base Information

Chemical Name:2-Phenylspiro[cyclopropane-1,9'-fluorene]
CAS No.:10423-18-4
Molecular Formula:C21H16
Molecular Weight:268.358
Hs Code.:
DSSTox Substance ID:DTXSID80533028
Nikkaji Number:J3.077.240G

Synonyms:2-PHENYLSPIRO[CYCLOPROPANE-1,9'-FLUORENE];10423-18-4;DTXSID80533028

Suppliers and Price of 2-Phenylspiro[cyclopropane-1,9'-fluorene]

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of 2-Phenylspiro[cyclopropane-1,9'-fluorene]

Chemical Property:

XLogP3:5.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:1
Exact Mass:268.125200510
Heavy Atom Count:21
Complexity:369

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1C(C12C3=CC=CC=C3C4=CC=CC=C24)C5=CC=CC=C5

Technology Process of 2-Phenylspiro[cyclopropane-1,9'-fluorene]

There total 19 articles about 2-Phenylspiro[cyclopropane-1,9'-fluorene] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 832-80-4
9-diazofluorenone

: 10423-18-4
2-phenylspiro[cyclopropane-1,9'-fluorene]

Guidance literature:: Irradiation;
DOI:10.1021/ja00319a037

Reference yield: 84.0%

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 13629-22-6
fluoren-9-ylidene-hydrazine

: 10423-18-4
2-phenylspiro[cyclopropane-1,9'-fluorene]

Guidance literature:: With iodosylbenzene; nickel(II) hydroxide; In neat (no solvent); at 80 ℃; for 2h;
DOI:10.1039/c5nj02378e

Reference yield: 69.0%

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 832-80-4
9-diazofluorenone

: 2071-44-5
di-fluoren-9-ylidene-hydrazine

: 10423-18-4
2-phenylspiro[cyclopropane-1,9'-fluorene]

Guidance literature:: pentacarbonyl(η²-cis-cyclooctene)chromium(0); In dichloromethane; for 16h; Ambient temperature;
DOI:10.1002/(SICI)1099-0690(199806)1998:6<1011::AID-EJOC1011>3.0.CO;2-H