C₆₀H₅₀O₁₆S

Base Information

Chemical Name:C₆₀H₅₀O₁₆S
CAS No.:1439439-44-7
Molecular Formula:C₆₀H₅₀O₁₆S
Molecular Weight:1059.11
Hs Code.:

C<sub>60</sub>H<sub>50</sub>O<sub>16</sub>S

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₆₀H₅₀O₁₆S

Chemical Property:

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Technology Process of C₆₀H₅₀O₁₆S

There total 5 articles about C₆₀H₅₀O₁₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1439439-41-4
phenyl 2,4-di-O-benzoyl-1-thio-α-D-mannopyranoside

: 183901-63-5
2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl trichloroacetimidate

: 1439439-44-7
C₆₀H₅₀O₁₆S

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -80 - 0 ℃; for 1.25h; regioselective reaction; Molecular sieve;
DOI:10.1039/c3ob40421h

Reference yield:

: 262605-68-5
phenyl 6-O-triphenylmethyl-1-thio-α-D-mannopyranoside

: 1439439-44-7
C₆₀H₅₀O₁₆S

Guidance literature:: Multi-step reaction with 5 steps

1.1: di(n-butyl)tin oxide / toluene / 3 h / 110 °C

1.2: 24 h / 20 °C

2.1: pyridine / 2 h / 50 °C

3.1: acetic acid / water / 3 h / 80 °C

4.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone; water / methanol; dichloromethane / 24 h / 20 °C

5.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 1.25 h / -80 - 0 °C / Molecular sieve

With pyridine; trimethylsilyl trifluoromethanesulfonate; water; di(n-butyl)tin oxide; acetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In methanol; dichloromethane; water; toluene;
DOI:10.1039/c3ob40421h

Reference yield:

: C₄₂H₃₈O₅S

: 1439439-44-7
C₆₀H₅₀O₁₆S

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / 2 h / 50 °C

2: acetic acid / water / 3 h / 80 °C

3: 2,3-dicyano-5,6-dichloro-p-benzoquinone; water / methanol; dichloromethane / 24 h / 20 °C

4: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 1.25 h / -80 - 0 °C / Molecular sieve

With pyridine; trimethylsilyl trifluoromethanesulfonate; water; acetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In methanol; dichloromethane; water;
DOI:10.1039/c3ob40421h