C₂₃H₂₅NO

Base Information

Chemical Name:C₂₃H₂₅NO
CAS No.:1616967-62-4
Molecular Formula:C₂₃H₂₅NO
Molecular Weight:331.458
Hs Code.:

Synonyms:

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Chemical Property of C₂₃H₂₅NO

Chemical Property:

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Technology Process of C₂₃H₂₅NO

There total 8 articles about C₂₃H₂₅NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1616967-63-5
C₂₀H₁₇NO₃S

: 104846-78-8
3,7-dimethyl-oct-6-en-1-yn-3-yl methyl carbonate

: 26871-46-5,28305-77-3,28305-78-4
mahanimbicine

: 1616967-62-4
C₂₃H₂₅NO

Guidance literature:: C₂₀H₁₇NO₃S; 3,7-dimethyl-oct-6-en-1-yn-3-yl methyl carbonate; With copper(l) iodide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile; at 20 ℃; for 22h; Inert atmosphere;

In 5,5-dimethyl-1,3-cyclohexadiene; for 27.5h; Inert atmosphere; Reflux;

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 70 - 75 ℃; for 6h; Inert atmosphere; Microwave irradiation;
DOI:10.1039/c4ob01151a

Reference yield:

: 2398-37-0
3-methoxyphenyl bromide

: 26871-46-5,28305-77-3,28305-78-4
mahanimbicine

: 1616967-62-4
C₂₃H₂₅NO

Guidance literature:: Multi-step reaction with 5 steps

1.1: palladium diacetate; caesium carbonate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / toluene / 17.5 h / Reflux; Inert atmosphere

2.1: palladium diacetate; potassium carbonate; Trimethylacetic acid / 20.5 h / 100 °C / Inert atmosphere

3.1: sodium hydride / tetrahydrofuran; mineral oil / 1.25 h / 0 °C / Inert atmosphere

3.2: 16.25 h / 0 - 20 °C / Inert atmosphere

4.1: boron tribromide / dichloromethane / 2.5 h / -78 - 20 °C / Inert atmosphere

4.2: Inert atmosphere

5.1: 1,8-diazabicyclo[5.4.0]undec-7-ene; copper(l) iodide / acetonitrile / 22 h / 20 °C / Inert atmosphere

5.2: 27.5 h / Inert atmosphere; Reflux

5.3: 6 h / 70 - 75 °C / Inert atmosphere; Microwave irradiation

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; copper(l) iodide; palladium diacetate; boron tribromide; sodium hydride; potassium carbonate; caesium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; Trimethylacetic acid; In tetrahydrofuran; dichloromethane; toluene; acetonitrile; mineral oil;
DOI:10.1039/c4ob01151a

Reference yield:

: 123017-90-3
N-(3-methoxyphenyl)-4-methylaniline

: 26871-46-5,28305-77-3,28305-78-4
mahanimbicine

: 1616967-62-4
C₂₃H₂₅NO

Guidance literature:: Multi-step reaction with 4 steps

1.1: palladium diacetate; potassium carbonate; Trimethylacetic acid / 20.5 h / 100 °C / Inert atmosphere

2.1: sodium hydride / tetrahydrofuran; mineral oil / 1.25 h / 0 °C / Inert atmosphere

2.2: 16.25 h / 0 - 20 °C / Inert atmosphere

3.1: boron tribromide / dichloromethane / 2.5 h / -78 - 20 °C / Inert atmosphere

3.2: Inert atmosphere

4.1: 1,8-diazabicyclo[5.4.0]undec-7-ene; copper(l) iodide / acetonitrile / 22 h / 20 °C / Inert atmosphere

4.2: 27.5 h / Inert atmosphere; Reflux

4.3: 6 h / 70 - 75 °C / Inert atmosphere; Microwave irradiation

With copper(l) iodide; palladium diacetate; boron tribromide; sodium hydride; potassium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; Trimethylacetic acid; In tetrahydrofuran; dichloromethane; acetonitrile; mineral oil;
DOI:10.1039/c4ob01151a