C₂₅H₁₇ClO₇

Base Information

Chemical Name:C₂₅H₁₇ClO₇
CAS No.:1616873-17-6
Molecular Formula:C₂₅H₁₇ClO₇
Molecular Weight:464.859
Hs Code.:

C<sub>25</sub>H<sub>17</sub>ClO<sub>7</sub>

Synonyms:

Suppliers and Price of C₂₅H₁₇ClO₇

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₅H₁₇ClO₇

Chemical Property:

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Technology Process of C₂₅H₁₇ClO₇

There total 15 articles about C₂₅H₁₇ClO₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1616873-11-0
C₂₇H₂₃ClO₇

: 1616873-17-6
C₂₅H₁₇ClO₇

Guidance literature:: With ammonium cerium (IV) nitrate; In water; ethyl acetate; acetonitrile; at 0 ℃; for 1.25h;
DOI:10.1002/chem.201402254

Reference yield:

: C₂₅H₃₃ClO₉

: 1616873-17-6
C₂₅H₁₇ClO₇

Guidance literature:: Multi-step reaction with 8 steps

1.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 20 h / 65 °C / Inert atmosphere

2.1: sodium acetate; acetic acid / 12 h / 80 °C / Inert atmosphere

3.1: hydrogenchloride; water / methanol; tetrahydrofuran / 16 h / 50 °C

4.1: toluene-4-sulfonic acid / acetone / 0.33 h / Inert atmosphere

4.2: 0.33 h

5.1: triethylamine; dmap / dichloromethane / 2 h / 0 °C / Inert atmosphere

6.1: hydrogenchloride; water / methanol; tetrahydrofuran / 16 h / 50 °C

7.1: methanesulfonyl chloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 °C / Inert atmosphere

7.2: 1 h / 0 °C / Inert atmosphere

8.1: ammonium cerium (IV) nitrate / water; ethyl acetate; acetonitrile / 1.25 h / 0 °C

With hydrogenchloride; dmap; ammonium cerium (IV) nitrate; water; sodium acetate; toluene-4-sulfonic acid; acetic acid; methanesulfonyl chloride; triethylamine; N-ethyl-N,N-diisopropylamine; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; acetone; acetonitrile;
DOI:10.1002/chem.201402254

Reference yield:

: 1616873-07-4
C₃₀H₂₉ClO₈

: 1616873-17-6
C₂₅H₁₇ClO₇

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride; water / methanol; tetrahydrofuran / 16 h / 50 °C

2.1: methanesulfonyl chloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 °C / Inert atmosphere

2.2: 1 h / 0 °C / Inert atmosphere

3.1: ammonium cerium (IV) nitrate / water; ethyl acetate; acetonitrile / 1.25 h / 0 °C

With hydrogenchloride; ammonium cerium (IV) nitrate; water; methanesulfonyl chloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; acetonitrile;
DOI:10.1002/chem.201402254