Technology Process of C27H48O4Si
There total 6 articles about C27H48O4Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
N-methyl-2-indolinone; tetrapropylammonium perruthennate;
In
dichloromethane;
at 0 - 20 ℃;
for 1h;
DOI:10.1016/j.bmcl.2007.05.037
- Guidance literature:
-
Multi-step reaction with 4 steps
1: Et3N; CuI / PdCl2(PPh3)2 / 80 °C
2: H2 / Pd/C / ethanol / 24 h / 20 °C
3: LiAlH4 / tetrahydrofuran / 2 h / 0 - 20 °C
4: TPAP; NMO / CH2Cl2 / 1 h / 0 - 20 °C
With
copper(l) iodide; lithium aluminium tetrahydride; N-methyl-2-indolinone; tetrapropylammonium perruthennate; hydrogen; triethylamine;
bis-triphenylphosphine-palladium(II) chloride; palladium on activated charcoal;
In
tetrahydrofuran; ethanol; dichloromethane;
1: Sonogashira cross-coupling / 4: Ley oxidation;
DOI:10.1016/j.bmcl.2007.05.037
- Guidance literature:
-
Multi-step reaction with 3 steps
1: H2 / Pd/C / ethanol / 24 h / 20 °C
2: LiAlH4 / tetrahydrofuran / 2 h / 0 - 20 °C
3: TPAP; NMO / CH2Cl2 / 1 h / 0 - 20 °C
With
lithium aluminium tetrahydride; N-methyl-2-indolinone; tetrapropylammonium perruthennate; hydrogen;
palladium on activated charcoal;
In
tetrahydrofuran; ethanol; dichloromethane;
3: Ley oxidation;
DOI:10.1016/j.bmcl.2007.05.037
