C₁₃H₁₆⁽²⁾HNO

Base Information

• Chemical Name: C₁₃H₁₆⁽²⁾HNO
• CAS No.: 85432-92-4
• Molecular Formula: C₁₃H₁₇NO
• Molecular Weight: 204.276
• Mol file: 85432-92-4.mol

Synonyms:

Chemical Property of C₁₃H₁₆⁽²⁾HNO

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₃H₁₆⁽²⁾HNO

There total 4 articles about C₁₃H₁₆⁽²⁾HNO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(tert-butyl)-3-phenyl-2-propenamide (99564-46-2) → C13H16(2)HNO (85432-92-4,85445-07-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 87 percent / D₂ / tris-triphenylphosphinerhodium chloride / benzene / 48 h

2: Cu(o-phen)2Cl₂, di-t-butylperoxide / chlorobenzene / 96 h / Heating

With di-tert-butyl peroxide; Cu(o-phen)2Cl₂; deuterium; tris(triphenylphosphine)rhodium(l) chloride; In chlorobenzene; benzene;

DOI:10.1016/0040-4020(82)85003-5

Reference yield:

N-(tert-butyl)-3-phenyl-2-propenamide (99564-46-2) → C13H16(2)HNO (85432-92-4,85445-07-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 87 percent / D₂ / tris-triphenylphosphinerhodium chloride / benzene / 48 h

2: Cu(o-phen)2Cl₂, di-t-butylperoxide / chlorobenzene / 96 h / Heating

With di-tert-butyl peroxide; Cu(o-phen)2Cl₂; deuterium; tris(triphenylphosphine)rhodium(l) chloride; In chlorobenzene; benzene;

DOI:10.1016/0040-4020(82)85003-5

Reference yield:

(+/-)-2,3-dideutero-N-t-butylcinnamamide (85432-93-5) → C13H16(2)HNO (85432-92-4,85445-07-4) + C13H16(2)HNO (85432-92-4,85445-07-4) + C13H15(2)H2NO (85432-90-2,85432-91-3) + C13H15(2)H2NO (85432-90-2,85432-91-3)

Guidance literature:

With di-tert-butyl peroxide; Cu(o-phen)2Cl₂; In chlorobenzene; for 96h; Title compound not separated from byproducts; Heating;

DOI:10.1016/0040-4020(82)85003-5

upstream raw materials:

(+/-)-2,3-dideutero-N-t-butylcinnamamide

N-(tert-butyl)-3-phenyl-2-propenamide