C₆₈H₉₀N₆O₁₂

Base Information

• Chemical Name: C₆₈H₉₀N₆O₁₂
• CAS No.: 1446713-59-2
• Molecular Formula: C₆₈H₉₀N₆O₁₂
• Molecular Weight: 1183.5
• Mol file: 1446713-59-2.mol

Synonyms:

Chemical Property of C₆₈H₉₀N₆O₁₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₆₈H₉₀N₆O₁₂

There total 6 articles about C₆₈H₉₀N₆O₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.5%

C27H45N3O4 (1446713-58-1) + 1,4,5,8-naphthalenetetracarboxylic dianhydride (81-30-1) → C68H90N6O12 (1446713-59-2)

Guidance literature:

In N,N-dimethyl-formamide; at 140 ℃; for 12h; Inert atmosphere;

DOI:10.1039/c3cc43538e

Reference yield:

C32H53N3O6 (1446713-57-0) → C68H90N6O12 (1446713-59-2)

Guidance literature:

Multi-step reaction with 2 steps

1: trifluoroacetic acid / 8 h

2: N,N-dimethyl-formamide / 12 h / 140 °C / Inert atmosphere

With trifluoroacetic acid; In N,N-dimethyl-formamide;

DOI:10.1039/c3cc43538e

Reference yield:

11-aminoundecanoic acid (2432-99-7,25587-80-8,84029-94-7) → C68H90N6O12 (1446713-59-2)

Guidance literature:

Multi-step reaction with 6 steps

1.1: sodium hydroxide / 1,4-dioxane; water / 20 °C / Cooling with ice

2.1: dicyclohexyl-carbodiimide; benzotriazol-1-ol / N,N-dimethyl-formamide / 20 °C / Cooling with ice

3.1: sodium hydroxide / methanol / 10 h

3.2: pH 2

4.1: dicyclohexyl-carbodiimide; benzotriazol-1-ol / N,N-dimethyl-formamide / 20 °C / Cooling with ice

5.1: trifluoroacetic acid / 8 h

6.1: N,N-dimethyl-formamide / 12 h / 140 °C / Inert atmosphere

With benzotriazol-1-ol; dicyclohexyl-carbodiimide; trifluoroacetic acid; sodium hydroxide; In 1,4-dioxane; methanol; water; N,N-dimethyl-formamide;

DOI:10.1039/c3cc43538e

upstream raw materials:

C₃₂H₅₃N₃O₆

C₂₇H₄₅N₃O₄

1,4,5,8-naphthalenetetracarboxylic dianhydride

11-(tert-butoxycarbonylamino)undecanoic acid