3-oxo-2-[5'-(2-oxo-1-phenylazo-1-phenylcarbamoyl-propylsulfanyl)-4,4'-diphenyl-4H,4'H-[3,3']bi[[1,2,4]triazolyl]-5-ylsulfanyl]-N-phenyl-2-phenylazo-butyramide

Base Information

• Chemical Name: 3-oxo-2-[5'-(2-oxo-1-phenylazo-1-phenylcarbamoyl-propylsulfanyl)-4,4'-diphenyl-4H,4'H-[3,3']bi[[1,2,4]triazolyl]-5-ylsulfanyl]-N-phenyl-2-phenylazo-butyramide
• CAS No.: 876595-87-8
• Molecular Formula: C₄₈H₃₈N₁₂O₄S₂
• Molecular Weight: 911.04

Synonyms:

Chemical Property of 3-oxo-2-[5'-(2-oxo-1-phenylazo-1-phenylcarbamoyl-propylsulfanyl)-4,4'-diphenyl-4H,4'H-[3,3']bi[[1,2,4]triazolyl]-5-ylsulfanyl]-N-phenyl-2-phenylazo-butyramide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 3-oxo-2-[5'-(2-oxo-1-phenylazo-1-phenylcarbamoyl-propylsulfanyl)-4,4'-diphenyl-4H,4'H-[3,3']bi[[1,2,4]triazolyl]-5-ylsulfanyl]-N-phenyl-2-phenylazo-butyramide

There total 2 articles about 3-oxo-2-[5'-(2-oxo-1-phenylazo-1-phenylcarbamoyl-propylsulfanyl)-4,4'-diphenyl-4H,4'H-[3,3']bi[[1,2,4]triazolyl]-5-ylsulfanyl]-N-phenyl-2-phenylazo-butyramide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,3'-bis(4-phenyl-1,2,4-triazole-5-thione) (49820-66-8) → 3-oxo-2-[5'-(2-oxo-1-phenylazo-1-phenylcarbamoyl-propylsulfanyl)-4,4'-diphenyl-4H,4'H-[3,3']bi[[1,2,4]triazolyl]-5-ylsulfanyl]-N-phenyl-2-phenylazo-butyramide (876595-87-8)

Guidance literature:

Multi-step reaction with 2 steps

1.1: 70 percent / sodium ethoxide / ethanol / 15 h / 20 °C

2.1: hydrochloric acid; sodium nitrite / H₂O

2.2: 85 percent / sodium acetate trihydrate / ethanol; H₂O / 0.5 h / cooling

With hydrogenchloride; sodium ethanolate; sodium nitrite; In ethanol; water;

Reference yield:

2-chloro-N-phenyl-3-oxobutanamide (31844-92-5,119878-78-3) → 3-oxo-2-[5'-(2-oxo-1-phenylazo-1-phenylcarbamoyl-propylsulfanyl)-4,4'-diphenyl-4H,4'H-[3,3']bi[[1,2,4]triazolyl]-5-ylsulfanyl]-N-phenyl-2-phenylazo-butyramide (876595-87-8)

Guidance literature:

Multi-step reaction with 2 steps

1.1: 70 percent / sodium ethoxide / ethanol / 15 h / 20 °C

2.1: hydrochloric acid; sodium nitrite / H₂O

2.2: 85 percent / sodium acetate trihydrate / ethanol; H₂O / 0.5 h / cooling

With hydrogenchloride; sodium ethanolate; sodium nitrite; In ethanol; water;

Reference yield:

3-oxo-2-[5'-(2-oxo-1-phenylazo-1-phenylcarbamoyl-propylsulfanyl)-4,4'-diphenyl-4H,4'H-[3,3']bi[[1,2,4]triazolyl]-5-ylsulfanyl]-N-phenyl-2-phenylazo-butyramide (876595-87-8) → 2-{N'-[4,4'-diphenyl-5'-(N-phenyl-N'-phenylaminothioxoacetyl-hydrazino)-4H,4'H-[3,3']bi[[1,2,4]triazolyl]-5-yl]-N'-phenyl-hydrazino}-N-phenyl-2-thioxo-acetamide

Guidance literature:

With sodium ethanolate; In ethanol; at 20 ℃; for 12h;

upstream raw materials:

3,3'-bis(4-phenyl-1,2,4-triazole-5-thione)

2-chloro-N-phenyl-3-oxobutanamide

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