C₄₈H₄₆N₂O₄

Base Information

• Chemical Name: C₄₈H₄₆N₂O₄
• CAS No.: 1354328-29-2
• Molecular Formula: C₄₈H₄₆N₂O₄
• Molecular Weight: 714.904
• Mol file: 1354328-29-2.mol

Synonyms:

Chemical Property of C₄₈H₄₆N₂O₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₈H₄₆N₂O₄

There total 8 articles about C₄₈H₄₆N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

→ C48H46N2O4 (1354328-29-2)

Guidance literature:

In methanol; at 20 ℃; for 3h;

Reference yield:

C16H18N2O2 → C48H46N2O4 (1354328-29-2)

Guidance literature:

Multi-step reaction with 2 steps

1: palladium on activated charcoal; hydrogen / methanol / 3 h / 20 °C

2: methanol / 3 h / 20 °C / Inert atmosphere

With palladium on activated charcoal; hydrogen; In methanol;

DOI:10.1021/ml200278u

Reference yield:

4-methyl-benzaldehyde (104-87-0) → C48H46N2O4 (1354328-29-2)

Guidance literature:

Multi-step reaction with 3 steps

1: formic acid; sodium cyanoborohydride / methanol / 6 h / 20 °C / Inert atmosphere

2: palladium on activated charcoal; hydrogen / methanol / 3 h / 20 °C

3: methanol / 3 h / 20 °C / Inert atmosphere

With formic acid; palladium on activated charcoal; hydrogen; sodium cyanoborohydride; In methanol;

DOI:10.1021/ml200278u

upstream raw materials:

C₄₀H₃₆O₅

4-methylbenzylhydrazine

4-methyl-benzaldehyde

trityl chloride

Downstream raw materials:

C₆₃H₆₅N₅O₈