Technology Process of C47H39BF2N2O4Se2
There total 6 articles about C47H39BF2N2O4Se2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: hydrogenchloride; water / dichloromethane / Cooling with ice
2: piperidine / toluene / 24 h / 135 °C / Inert atmosphere
3: hypobromous acid / acetonitrile; water / 0.5 h
With
piperidine; hydrogenchloride; water; hypobromous acid;
In
dichloromethane; water; toluene; acetonitrile;
DOI:10.1039/c3cc42313a
- Guidance literature:
-
With
hypobromous acid;
In
water; acetonitrile;
for 0.5h;
DOI:10.1039/c3cc42313a
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: toluene-4-sulfonic acid / toluene / 10 h / Reflux; Dean-Stark
2.1: magnesium / tetrahydrofuran
2.2: 2 h / Reflux
3.1: hydrogenchloride; water / dichloromethane / Cooling with ice
4.1: piperidine / toluene / 24 h / 135 °C / Inert atmosphere
5.1: hypobromous acid / acetonitrile; water / 0.5 h
With
piperidine; hydrogenchloride; water; hypobromous acid; toluene-4-sulfonic acid; magnesium;
In
tetrahydrofuran; dichloromethane; water; toluene; acetonitrile;
DOI:10.1039/c3cc42313a