C₃₂H₄₄ClN₅O₇S

Base Information

Chemical Name:C₃₂H₄₄ClN₅O₇S
CAS No.:1415413-53-4
Molecular Formula:C₃₂H₄₄ClN₅O₇S
Molecular Weight:678.25
Hs Code.:

C<sub>32</sub>H<sub>44</sub>ClN<sub>5</sub>O<sub>7</sub>S

Synonyms:

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Chemical Property of C₃₂H₄₄ClN₅O₇S

Chemical Property:

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Technology Process of C₃₂H₄₄ClN₅O₇S

There total 18 articles about C₃₂H₄₄ClN₅O₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 944142-39-6
(2R)-1-ethoxy-4-methylpentan-2-amine

: 1263198-07-7
(3S,5R)-5-[4-(2-chlorophenyl)-2,2-dimethyl-5-oxopiperazin-1-yl]-1-(2-nitrophenyl)sulfonylpiperidine-3-carboxylic acid

: 1415413-53-4
C₃₂H₄₄ClN₅O₇S

Guidance literature:: With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 5h;
DOI:10.1016/j.bmcl.2012.09.103

Reference yield:

: 2,4-dioxo-3-oxa-7-azabicyclo[3.3.1]nonane-7-carboxylic acid tert-butyl ester

: 1415413-53-4
C₃₂H₄₄ClN₅O₇S

Guidance literature:: Multi-step reaction with 15 steps

1: C₂₈H₂₇F₆N₃O₃S / tetrahydrofuran / 24 h / -20 °C

2: diphenylphosphoranyl azide; triethylamine / toluene / 15 h / 90 °C

3: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

4: triethylamine / dichloromethane / 1 h / 20 °C

5: tetrakis(triphenylphosphine) palladium⁽⁰⁾; morpholine / tetrahydrofuran / 1 h / 20 °C

6: dichloromethane / 2 h / 20 °C

7: N-chloro-succinimide / dichloromethane / 2 h / 20 °C

8: 18 h / 60 °C

9: hydrogenchloride / dichloromethane; water / 4 h / 40 °C

10: thionyl chloride / 1 h / 20 °C

11: acetic acid / toluene / 2 h / 110 °C

12: sodium cyanoborohydride / 6 h / 20 °C

13: triethylamine / dichloromethane / 5 h / 0 - 40 °C

14: sodium hydroxide; water / methanol / 0.5 h / 50 °C

15: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 5 h / 20 °C

With morpholine; hydrogenchloride; N-chloro-succinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; thionyl chloride; C₂₈H₂₇F₆N₃O₃S; diphenylphosphoranyl azide; water; sodium cyanoborohydride; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; 2: |Curtius Rearrangement;
DOI:10.1016/j.bmcl.2012.09.103

Reference yield:

: 1415413-38-5
C₁₆H₂₆N₂O₆

: 1415413-53-4
C₃₂H₄₄ClN₅O₇S

Guidance literature:: Multi-step reaction with 13 steps

1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

2: triethylamine / dichloromethane / 1 h / 20 °C

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; morpholine / tetrahydrofuran / 1 h / 20 °C

4: dichloromethane / 2 h / 20 °C

5: N-chloro-succinimide / dichloromethane / 2 h / 20 °C

6: 18 h / 60 °C

7: hydrogenchloride / dichloromethane; water / 4 h / 40 °C

8: thionyl chloride / 1 h / 20 °C

9: acetic acid / toluene / 2 h / 110 °C

10: sodium cyanoborohydride / 6 h / 20 °C

11: triethylamine / dichloromethane / 5 h / 0 - 40 °C

12: sodium hydroxide; water / methanol / 0.5 h / 50 °C

13: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 5 h / 20 °C

With morpholine; hydrogenchloride; N-chloro-succinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; thionyl chloride; water; sodium cyanoborohydride; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.bmcl.2012.09.103