1-deuterio-2-phenylclopropylamine hydrochloride

Base Information

Chemical Name:1-deuterio-2-phenylclopropylamine hydrochloride
CAS No.:92456-25-2
Molecular Formula:C₉H₁₁N*ClH
Molecular Weight:170.646
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-deuterio-2-phenylclopropylamine hydrochloride

Chemical Property:

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Technology Process of 1-deuterio-2-phenylclopropylamine hydrochloride

There total 4 articles about 1-deuterio-2-phenylclopropylamine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4660-02-0
2-phenylcyclopropane-1-carbonitrile

: 92456-25-2
1-deuterio-2-phenylclopropylamine hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) NaOMe, 2.) NaOD, D₂O / 1.) methanol-d, reflux, 2.) reflux, 6 h

2: SOCl₂ / toluene / 6 h / 60 °C

3: NaN₃ / toluene / Heating

4: 4N HCl / 10 h / Heating

With hydrogenchloride; thionyl chloride; sodium azide; deuteriated sodium hydroxide; water-d2; sodium methylate; In toluene;
DOI:10.1021/jo00197a056

Reference yield:

: C₁₀H₈⁽²⁾HClO

: 92456-25-2
1-deuterio-2-phenylclopropylamine hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: NaN₃ / toluene / Heating

2: 4N HCl / 10 h / Heating

With hydrogenchloride; sodium azide; In toluene;
DOI:10.1021/jo00197a056

Reference yield:

: 92456-24-1
1-deuterio-2-phenylclopropanecarboxylic acid

: 92456-25-2
1-deuterio-2-phenylclopropylamine hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: SOCl₂ / toluene / 6 h / 60 °C

2: NaN₃ / toluene / Heating

3: 4N HCl / 10 h / Heating

With hydrogenchloride; thionyl chloride; sodium azide; In toluene;
DOI:10.1021/jo00197a056