Benzoic acid, 2-[(tetrahydro-2-furanyl)thio]-, tetrahydro-2-furanyl ester

Base Information

Chemical Name:Benzoic acid, 2-[(tetrahydro-2-furanyl)thio]-, tetrahydro-2-furanyl ester
CAS No.:104324-44-9
Molecular Formula:C15H18O4S
Molecular Weight:294.372
Hs Code.:

Synonyms:2-(Tetrahydro-furan-2-ylsulfanyl)-benzoic acid tetrahydro-furan-2-yl ester;

Suppliers and Price of Benzoic acid, 2-[(tetrahydro-2-furanyl)thio]-, tetrahydro-2-furanyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Benzoic acid, 2-[(tetrahydro-2-furanyl)thio]-, tetrahydro-2-furanyl ester

Chemical Property:

PSA：70.06000
LogP:3.20850

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzoic acid, 2-[(tetrahydro-2-furanyl)thio]-, tetrahydro-2-furanyl ester

There total 1 articles about Benzoic acid, 2-[(tetrahydro-2-furanyl)thio]-, tetrahydro-2-furanyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 13369-70-5
2-chlorotetrahydrofuran

: 147-93-3
Thiosalicylic acid

: 104324-44-9
2-tetrahydrofuranyl o-(2-tetrahydrofuranylthio)benzoate

Guidance literature:: With triethylamine; In tetrahydrofuran; for 2.5h; Ambient temperature;
DOI:10.1021/ja00282a033

Reference yield: 93.0%

: 104324-44-9
2-tetrahydrofuranyl o-(2-tetrahydrofuranylthio)benzoate

: 104324-45-0
o-(2-tetrahydrofuranylthio)benzyl alcohol

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; for 8h; Ambient temperature;
DOI:10.1021/ja00282a033

Reference yield:

: 104324-44-9
2-tetrahydrofuranyl o-(2-tetrahydrofuranylthio)benzoate

: 104324-58-5
2-Propylsulfanylmethyl-benzenethiol

Guidance literature:: Multi-step reaction with 4 steps

1: 93 percent / lithium aluminum hydride / diethyl ether / 8 h / Ambient temperature

2: 91 percent / triethylamine / CH₂Cl₂ / 0.17 h / -10 °C

3: tetrahydrofuran / 0.5 h / Ambient temperature

4: 1.) silver nitrate; 2.) hydrogen sulfide / 1.) water, methanol, heating, 10 min; 2.) methylene chloride, 5 min

With lithium aluminium tetrahydride; hydrogen sulfide; silver nitrate; triethylamine; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/ja00282a033