Technology Process of Disulfide, 2-propenyl 2-[(2-propenylsulfinyl)methyl]phenyl
There total 7 articles about Disulfide, 2-propenyl 2-[(2-propenylsulfinyl)methyl]phenyl which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid;
In
dichloromethane;
for 0.166667h;
Ambient temperature;
DOI:10.1021/ja00282a033
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 90 percent / triethylamine / tetrahydrofuran / 2.5 h / Ambient temperature
2: 93 percent / lithium aluminum hydride / diethyl ether / 8 h / Ambient temperature
3: 91 percent / triethylamine / CH2Cl2 / 0.17 h / -10 °C
4: 87 percent / tetrahydrofuran / 0.5 h / Ambient temperature
5: 1.) silver nitrate; 2.) hydrogen sulfide / 1.) water, methanol, heating, 10 min; 2.) methylene chloride, 5 min
6: 97 percent / 1.) n-butyllithium / hexane; tetrahydrofuran / 0.5 h / Ambient temperature
7: 81 percent / 1.) 80 percent MCPBA; 2.) 5 percent sodium bicarbonate / CH2Cl2 / 0.17 h / Ambient temperature
With
lithium aluminium tetrahydride; n-butyllithium; hydrogen sulfide; sodium hydrogencarbonate; silver nitrate; triethylamine; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; diethyl ether; hexane; dichloromethane;
DOI:10.1021/ja00282a033
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 97 percent / 1.) n-butyllithium / hexane; tetrahydrofuran / 0.5 h / Ambient temperature
2: 81 percent / 1.) 80 percent MCPBA; 2.) 5 percent sodium bicarbonate / CH2Cl2 / 0.17 h / Ambient temperature
With
n-butyllithium; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; hexane; dichloromethane;
DOI:10.1021/ja00282a033
