1-(4-nitrophenyl)-4-ferrocenylmethylenetetrazolium fluoroborate

Base Information

• Chemical Name: 1-(4-nitrophenyl)-4-ferrocenylmethylenetetrazolium fluoroborate
• CAS No.: 207301-19-7
• Molecular Formula: BF₄*C₁₈H₁₆FeN₅O₂
• Molecular Weight: 477.009
• Mol file: 207301-19-7.mol

Synonyms:

Chemical Property of 1-(4-nitrophenyl)-4-ferrocenylmethylenetetrazolium fluoroborate

Chemical Property:

Purity/Quality:

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Technology Process of 1-(4-nitrophenyl)-4-ferrocenylmethylenetetrazolium fluoroborate

There total 1 articles about 1-(4-nitrophenyl)-4-ferrocenylmethylenetetrazolium fluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

tetrafluoroboric acid + 1-ferrocenylmethanol (1273-86-5) + 5-(4-nitrophenyl)-1H-1,2,3,4-tetrazole (16687-60-8) → 1-(4-nitrophenyl)-4-ferrocenylmethylenetetrazolium fluoroborate (207301-19-7)

Guidance literature:

In dichloromethane; water; aq. soln. of HBF4 addn. to soln. of Fe-compd. and tetrazole in CH2Cl2 with vigorous stirring, reaction time 10 min; hexane-diethyl ether addn., ppt. filtration off, washing (cooled water),vacuum drying (over P2O5); elem. anal.;

Reference yield:

1-(4-nitrophenyl)-4-ferrocenylmethylenetetrazolium fluoroborate (207301-19-7) → 1-ferrocenylmethanol (1273-86-5) + 5-(4-nitrophenyl)-1H-1,2,3,4-tetrazole (16687-60-8)

Guidance literature:

With sodium hydroxide; In water; refluxing (5-10 min), cooling to 5 to 7°C; ppt. filtration off, washing (hot pentane), Fe-compd. obtaining from pentane extracts by drying, tetrazole remaining in the solid residue;

upstream raw materials:

1-ferrocenylmethanol

5-(4-nitrophenyl)-1H-1,2,3,4-tetrazole

Downstream raw materials:

1-ferrocenylmethanol

5-(4-nitrophenyl)-1H-1,2,3,4-tetrazole

Refernces