methyl di (3-sulfonatophenyl) phosphine oxide, diacid

Base Information

Chemical Name:methyl di (3-sulfonatophenyl) phosphine oxide, diacid
CAS No.:135265-28-0
Molecular Formula:C₁₃H₁₃O₇PS₂
Molecular Weight:376.348
Hs Code.:

Synonyms:

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Chemical Property of methyl di (3-sulfonatophenyl) phosphine oxide, diacid

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Technology Process of methyl di (3-sulfonatophenyl) phosphine oxide, diacid

There total 3 articles about methyl di (3-sulfonatophenyl) phosphine oxide, diacid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 96723-93-2
tris (3-sulfonatophenyl) phosphine oxide, triacid

: 135265-28-0
methyl di (3-sulfonatophenyl) phosphine oxide, diacid

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) Ag₂CO₃, aq. aerosol OT / 1.) 25 deg C, 24 h, 2.) toluene, reflux, 24 h

2: 89 percent / SiHCl₃ / toluene; tetrahydrofuran / 22 h / Heating

3: 66 percent / sodium bromide / H₂O; acetone / 48 h / Ambient temperature

4: 2.) NaOH / 1.) H₂O, RT, overnight, 2.) H₂O, reflux, 30 min

With sodium hydroxide; aerosol OT; trichlorosilane; silver carbonate; sodium bromide; In tetrahydrofuran; water; acetone; toluene;
DOI:10.1080/00397919108016775

Reference yield:

: 135265-27-9
tris (3-ethyl phenyl sulfonate) phosphine

: 135265-28-0
methyl di (3-sulfonatophenyl) phosphine oxide, diacid

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / sodium bromide / H₂O; acetone / 48 h / Ambient temperature

2: 2.) NaOH / 1.) H₂O, RT, overnight, 2.) H₂O, reflux, 30 min

With sodium hydroxide; sodium bromide; In water; acetone;
DOI:10.1080/00397919108016775

Reference yield:

: 135265-26-8
tris (3-ethyl phenyl sulfonate) phosphine oxide

: 135265-28-0
methyl di (3-sulfonatophenyl) phosphine oxide, diacid

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / SiHCl₃ / toluene; tetrahydrofuran / 22 h / Heating

2: 66 percent / sodium bromide / H₂O; acetone / 48 h / Ambient temperature

3: 2.) NaOH / 1.) H₂O, RT, overnight, 2.) H₂O, reflux, 30 min

With sodium hydroxide; trichlorosilane; sodium bromide; In tetrahydrofuran; water; acetone; toluene;
DOI:10.1080/00397919108016775