C₂₅H₃₄O₅Si

Base Information

Chemical Name:C₂₅H₃₄O₅Si
CAS No.:1600522-94-8
Molecular Formula:C₂₅H₃₄O₅Si
Molecular Weight:442.627
Hs Code.:

C<sub>25</sub>H<sub>34</sub>O<sub>5</sub>Si

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₅H₃₄O₅Si

Chemical Property:

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Technology Process of C₂₅H₃₄O₅Si

There total 5 articles about C₂₅H₃₄O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1600522-27-7
C₁₇H₂₂O₅

: 768-33-2
phenyldimethylsilyl chloride

: 1600522-94-8
C₂₅H₃₄O₅Si

Guidance literature:: phenyldimethylsilyl chloride; With lithium; In tetrahydrofuran; at 20 ℃; for 3h; Inert atmosphere;

C₁₇H₂₂O₅; In tetrahydrofuran; at -78 ℃; for 1h; Inert atmosphere;
DOI:10.1002/anie.201308824

Reference yield:

: 1600522-88-0
C₃₃H₄₂O₅Si

: 1600522-94-8
C₂₅H₃₄O₅Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

2.1: Dess-Martin periodane / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

3.1: lithium / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

3.2: 1 h / -78 °C / Inert atmosphere

With tetrabutyl ammonium fluoride; lithium; Dess-Martin periodane; In tetrahydrofuran; dichloromethane;
DOI:10.1002/anie.201308824

Reference yield:

: 1600522-89-1
C₁₇H₂₄O₅

: 1600522-94-8
C₂₅H₃₄O₅Si

Guidance literature:: Multi-step reaction with 2 steps

1.1: Dess-Martin periodane / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

2.1: lithium / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

2.2: 1 h / -78 °C / Inert atmosphere

With lithium; Dess-Martin periodane; In tetrahydrofuran; dichloromethane;
DOI:10.1002/anie.201308824