Benzenamine, 2-[(1H-benzimidazol-2-ylthio)methyl]-

Base Information

Chemical Name:Benzenamine, 2-[(1H-benzimidazol-2-ylthio)methyl]-
CAS No.:104340-33-2
Molecular Formula:C14H13N3S
Molecular Weight:255.343
Hs Code.:
DSSTox Substance ID:DTXSID70453549
Nikkaji Number:J386.969E
Mol file:104340-33-2.mol

Synonyms:104340-33-2;Benzenamine, 2-[(1H-benzimidazol-2-ylthio)methyl]-;SCHEMBL6480868;DTXSID70453549;VIDRTFCKVZQFTK-UHFFFAOYSA-N;AKOS000213821;2-[[2-[Amino]benzyl]thio]-1H-benzimidazole;2-[(1H-Benzimidazol-2-yl)thiomethyl]benzenamine;2-[(1H-Benzimidazol-2-ylthio)methyl]benzenamine

Suppliers and Price of Benzenamine, 2-[(1H-benzimidazol-2-ylthio)methyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenamine, 2-[(1H-benzimidazol-2-ylthio)methyl]-

Chemical Property:

XLogP3:3.1
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:255.08301860
Heavy Atom Count:18
Complexity:274

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C(=C1)CSC2=NC3=CC=CC=C3N2)N

Technology Process of Benzenamine, 2-[(1H-benzimidazol-2-ylthio)methyl]-

There total 5 articles about Benzenamine, 2-[(1H-benzimidazol-2-ylthio)methyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.4%

: 108499-76-9
2-<2-((benzyloxycarbonyl)aminobenzyl)thio>-1H-benzimidazole

: 104340-33-2
2-<(1H-benzimidazol-2-ylthio)methyl>aniline

Guidance literature:: With hydrogen bromide; acetic acid; for 3h; Ambient temperature;
DOI:10.1016/0223-5234(91)90024-H

Reference yield: 20.0%

: 5344-90-1
2-Aminobenzyl alcohol

: 134469-07-1
Benzimidazol-2-thiol

: 104340-33-2
2-<(1H-benzimidazol-2-ylthio)methyl>aniline

Guidance literature:: With sulfuric acid; In acetic acid; at 84 ℃; for 3h;
DOI:10.1021/jm00401a024

Reference yield:

: 5344-90-1
2-Aminobenzyl alcohol

: 104340-33-2
2-<(1H-benzimidazol-2-ylthio)methyl>aniline

Guidance literature:: Multi-step reaction with 4 steps

1: 82.4 percent / K₂CO₃ / CHCl₃ / 1.) 4 h, 2.) RT, overnight

2: SOCl₂ / benzene / 1 h / Heating

3: NaOH / H₂O; ethanol / 2 h / Ambient temperature

4: 84.4 percent / 30percent HBr-AcOH / 3 h / Ambient temperature

With sodium hydroxide; thionyl chloride; hydrogen bromide; potassium carbonate; acetic acid; In ethanol; chloroform; water; benzene;
DOI:10.1016/0223-5234(91)90024-H