(2R,3S)-2-allylbutane-1,3-diol 1-benzyl ether 3-tosylate

Base Information

Chemical Name:(2R,3S)-2-allylbutane-1,3-diol 1-benzyl ether 3-tosylate
CAS No.:113195-24-7
Molecular Formula:C₂₁H₂₆O₄S
Molecular Weight:374.501
Hs Code.:

Synonyms:

Suppliers and Price of (2R,3S)-2-allylbutane-1,3-diol 1-benzyl ether 3-tosylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2R,3S)-2-allylbutane-1,3-diol 1-benzyl ether 3-tosylate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2R,3S)-2-allylbutane-1,3-diol 1-benzyl ether 3-tosylate

There total 6 articles about (2R,3S)-2-allylbutane-1,3-diol 1-benzyl ether 3-tosylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 73574-05-7
(2S,1'S)-2-(1-hydroxyethyl)-pent-4-enoate d'ethyle

: 113195-24-7
(2R,3S)-2-allylbutane-1,3-diol 1-benzyl ether 3-tosylate

Guidance literature:: Multi-step reaction with 5 steps

1: pyridinium p-toluenesulfonate / CH₂Cl₂

2: 99.7 percent / LAH / diethyl ether

3: 59.7 g / NaH 60 percent , n-Bu₄N⁽¹⁺⁾*I^(1-) / paraffin; tetrahydrofuran / 3 h / Heating

4: p-TsOH*H₂O / methanol

5: DMAP / pyridine

With dmap; lithium aluminium tetrahydride; tetra-(n-butyl)ammonium iodide; sodium hydride; pyridinium p-toluenesulfonate; toluene-4-sulfonic acid; In tetrahydrofuran; pyridine; methanol; diethyl ether; dichloromethane; paraffin;
DOI:10.1016/S0040-4020(01)89929-4

Reference yield:

: 113195-22-5
(2R,3S)-2-allylbutane-1,3-diol 3-THP ether

: 113195-24-7
(2R,3S)-2-allylbutane-1,3-diol 1-benzyl ether 3-tosylate

Guidance literature:: Multi-step reaction with 3 steps

1: 59.7 g / NaH 60 percent , n-Bu₄N⁽¹⁺⁾*I^(1-) / paraffin; tetrahydrofuran / 3 h / Heating

2: p-TsOH*H₂O / methanol

3: DMAP / pyridine

With dmap; tetra-(n-butyl)ammonium iodide; sodium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; pyridine; methanol; paraffin;
DOI:10.1016/S0040-4020(01)89929-4

Reference yield:

: 113195-21-4
ethyl (2S,1'S)-2-(1'-tetrahydropyranyloxyethyl)pent-4-enoate

: 113195-24-7
(2R,3S)-2-allylbutane-1,3-diol 1-benzyl ether 3-tosylate

Guidance literature:: Multi-step reaction with 4 steps

1: 99.7 percent / LAH / diethyl ether

2: 59.7 g / NaH 60 percent , n-Bu₄N⁽¹⁺⁾*I^(1-) / paraffin; tetrahydrofuran / 3 h / Heating

3: p-TsOH*H₂O / methanol

4: DMAP / pyridine

With dmap; lithium aluminium tetrahydride; tetra-(n-butyl)ammonium iodide; sodium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; pyridine; methanol; diethyl ether; paraffin;
DOI:10.1016/S0040-4020(01)89929-4