Technology Process of C58H63N3O3S
There total 5 articles about C58H63N3O3S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
copper(l) chloride;
In
1,3,5-trimethyl-benzene;
for 20h;
Inert atmosphere;
Schlenk technique;
Reflux;
DOI:10.1039/c3ob42564a
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tetrabutyl ammonium fluoride / dichloromethane; tetrahydrofuran / 0.33 h
2: pyridine; copper diacetate / toluene / 96 h
3: copper(l) chloride / 1,3,5-trimethyl-benzene / 20 h / Inert atmosphere; Schlenk technique; Reflux
With
pyridine; tetrabutyl ammonium fluoride; copper diacetate; copper(l) chloride;
In
tetrahydrofuran; dichloromethane; toluene; 1,3,5-trimethyl-benzene;
2: |Glaser Coupling;
DOI:10.1039/c3ob42564a
- Guidance literature:
-
Multi-step reaction with 2 steps
1: pyridine; copper diacetate / toluene / 96 h
2: copper(l) chloride / 1,3,5-trimethyl-benzene / 20 h / Inert atmosphere; Schlenk technique; Reflux
With
pyridine; copper diacetate; copper(l) chloride;
In
toluene; 1,3,5-trimethyl-benzene;
1: |Glaser Coupling;
DOI:10.1039/c3ob42564a