1-(carbo-t-butoxymethyl)-4-(2-carboethoxyethyl)-7-[(4-amidinophenyl)methyl]-3,4-dihydro-1H-1,4-benzodiazepine-2,5-dione, acetate

Base Information

Chemical Name:1-(carbo-t-butoxymethyl)-4-(2-carboethoxyethyl)-7-[(4-amidinophenyl)methyl]-3,4-dihydro-1H-1,4-benzodiazepine-2,5-dione, acetate
CAS No.:301534-09-8
Molecular Formula:C₂H₄O₂*C₂₈H₃₄N₄O₆
Molecular Weight:582.654
Hs Code.:

Synonyms:

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Chemical Property of 1-(carbo-t-butoxymethyl)-4-(2-carboethoxyethyl)-7-[(4-amidinophenyl)methyl]-3,4-dihydro-1H-1,4-benzodiazepine-2,5-dione, acetate

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Technology Process of 1-(carbo-t-butoxymethyl)-4-(2-carboethoxyethyl)-7-[(4-amidinophenyl)methyl]-3,4-dihydro-1H-1,4-benzodiazepine-2,5-dione, acetate

There total 9 articles about 1-(carbo-t-butoxymethyl)-4-(2-carboethoxyethyl)-7-[(4-amidinophenyl)methyl]-3,4-dihydro-1H-1,4-benzodiazepine-2,5-dione, acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 301534-02-1
5-benzyloxyanthranilic acid, benzyl ester, hydrochloride

: 301534-09-8
1-(carbo-t-butoxymethyl)-4-(2-carboethoxyethyl)-7-[(4-amidinophenyl)methyl]-3,4-dihydro-1H-1,4-benzodiazepine-2,5-dione, acetate

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hydrogencarbonate / ethyl acetate; N,N-dimethyl-formamide

2: palladium-carbon / tetrahydrofuran; methanol; ethyl acetate

3: triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / palladium-carbon / methanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide

4: potassium carbonate / ethyl acetate; N,N-dimethyl-formamide

5: pyridine; ammonium acetate; sodium hydroxide; triethylamine / methanol; dichloromethane; acetone; toluene; acetonitrile

With pyridine; ammonium acetate; sodium hydroxide; sodium hydrogencarbonate; potassium carbonate; triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; palladium-carbon; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; acetone; toluene; acetonitrile;

Reference yield:

: 301534-05-4
3-[N-(benzyloxycarbonylmethyl)amino]propionic acid ethyl ester

: 301534-09-8
1-(carbo-t-butoxymethyl)-4-(2-carboethoxyethyl)-7-[(4-amidinophenyl)methyl]-3,4-dihydro-1H-1,4-benzodiazepine-2,5-dione, acetate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / palladium-carbon / methanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide

2: potassium carbonate / ethyl acetate; N,N-dimethyl-formamide

3: pyridine; ammonium acetate; sodium hydroxide; triethylamine / methanol; dichloromethane; acetone; toluene; acetonitrile

With pyridine; ammonium acetate; sodium hydroxide; potassium carbonate; triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; palladium-carbon; In methanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; acetone; toluene; acetonitrile;

Reference yield:

: 301534-04-3
N-(carbo-t-butoxymethyl)-5-hydroxyanthranilic acid

: 301534-09-8
1-(carbo-t-butoxymethyl)-4-(2-carboethoxyethyl)-7-[(4-amidinophenyl)methyl]-3,4-dihydro-1H-1,4-benzodiazepine-2,5-dione, acetate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / palladium-carbon / methanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide

2: potassium carbonate / ethyl acetate; N,N-dimethyl-formamide

3: pyridine; ammonium acetate; sodium hydroxide; triethylamine / methanol; dichloromethane; acetone; toluene; acetonitrile

With pyridine; ammonium acetate; sodium hydroxide; potassium carbonate; triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; palladium-carbon; In methanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; acetone; toluene; acetonitrile;