C₃₁H₃₈ClN₄O₁₅PS

Base Information

• Chemical Name: C₃₁H₃₈ClN₄O₁₅PS
• CAS No.: 79258-29-0
• Molecular Formula: C₃₁H₃₈ClN₄O₁₅PS
• Molecular Weight: 805.153
• Mol file: 79258-29-0.mol

Synonyms:

Chemical Property of C₃₁H₃₈ClN₄O₁₅PS

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of C₃₁H₃₈ClN₄O₁₅PS

There total 3 articles about C₃₁H₃₈ClN₄O₁₅PS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(methylthiomethoxy)ethoxycarbonyl chloride (79258-36-9) → C31H38ClN4O15PS (79258-29-0)

Guidance literature:

Multi-step reaction with 3 steps

1: 2.) p-toluenesulfonic acid / 1.) acetonitril, room temprature, 1 hr; 2.) CHCl₃-CH₃OH, 2 min

2: 83 percent / 1-(mesitylene 2-sulfonyl)-3-nitro-1,2,4-triazol / pyridine

3: 1.) silver perchlorate, 2,4,6-collidine; 2.) mopholine / 1.) acetone, water, room temp., 1 h

With morpholine; 2,4,6-trimethyl-pyridine; silver perchlorate; 1-(mesitylene-2-sulfonyl)-3-nitro-1H-1,2,4-triazole; toluene-4-sulfonic acid; In pyridine;

DOI:10.1016/S0040-4039(01)90482-4

Reference yield:

3'-O-(2-methylthiomethoxy)ethoxycarbonylthymidine (79258-35-8) → C31H38ClN4O15PS (79258-29-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 83 percent / 1-(mesitylene 2-sulfonyl)-3-nitro-1,2,4-triazol / pyridine

2: 1.) silver perchlorate, 2,4,6-collidine; 2.) mopholine / 1.) acetone, water, room temp., 1 h

With morpholine; 2,4,6-trimethyl-pyridine; silver perchlorate; 1-(mesitylene-2-sulfonyl)-3-nitro-1H-1,2,4-triazole; In pyridine;

DOI:10.1016/S0040-4039(01)90482-4

Reference yield:

C39H42Br2ClN4O16PS (79258-30-3) → C31H38ClN4O15PS (79258-29-0)

Guidance literature:

With morpholine; 2,4,6-trimethyl-pyridine; silver perchlorate; Yield given. Multistep reaction; 1.) acetone, water, room temp., 1 h;

DOI:10.1016/S0040-4039(01)90482-4

upstream raw materials:

C₃₉H₄₂Br₂ClN₄O₁₆PS

2-(methylthiomethoxy)ethoxycarbonyl chloride

3'-O-(2-methylthiomethoxy)ethoxycarbonylthymidine

Downstream raw materials:

C₇₁H₇₄Br₂Cl₃N₈O₃₀P₃S