Co⁽²⁺⁾*2COOHC₆H₄B(N₂C₃H₃)3^(1-)=Co(COOHC₆H₄B(N₂C₃H₃)3)2

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Chemical Name:Co⁽²⁺⁾*2COOHC₆H₄B(N₂C₃H₃)3^(1-)=Co(COOHC₆H₄B(N₂C₃H₃)3)2
CAS No.:80583-81-9
Molecular Formula:2C₁₆H₁₄BN₆O₂*Co
Molecular Weight:725.268
Hs Code.:

Co<sup>(2+)</sup>*2COOHC<sub>6</sub>H<sub>4</sub>B(N<sub>2</sub>C<sub>3</sub>H<sub>3</sub>)3<sup>(1-)</sup>=Co(COOHC<sub>6</sub>H<sub>4</sub>B(N<sub>2</sub>C<sub>3</sub>H<sub>3</sub>)3)2

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Chemical Property of Co⁽²⁺⁾*2COOHC₆H₄B(N₂C₃H₃)3^(1-)=Co(COOHC₆H₄B(N₂C₃H₃)3)2

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Technology Process of Co⁽²⁺⁾*2COOHC₆H₄B(N₂C₃H₃)3^(1-)=Co(COOHC₆H₄B(N₂C₃H₃)3)2

There total 1 articles about Co⁽²⁺⁾*2COOHC₆H₄B(N₂C₃H₃)3^(1-)=Co(COOHC₆H₄B(N₂C₃H₃)3)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 109-72-8,29786-93-4
n-butyllithium

: 80583-79-5
bis[(4-bromophenyl)tris(1-pyrazolyl)borato]cobalt(II)

: Co⁽²⁺⁾*2K⁽¹⁺⁾*2COOC₆H₄B(N₂C₃H₃)3^(2-)*2.5H₂O=CoK₂(COOC₆H₄B(N₂C₃H₃)3)2*2.5H₂O

: Co⁽²⁺⁾*COOHC₆H₄B(N₂C₃H₃)3^(1-)*C₆H₅B(N₂C₃H₃)3^(1-)=Co(COOHC₆H₄B(N₂C₃H₃)3)(C₆H₅B(N₂C₃H₃)3)

: 80583-81-9
Co⁽²⁺⁾*2COOHC₆H₄B(N₂C₃H₃)3^(1-)=Co(COOHC₆H₄B(N₂C₃H₃)3)2

Guidance literature:: With potassium hydroxide; carbon dioxide; acetic acid; In tetrahydrofuran; hexane; Co-complex was dissolved in THF, soln. was cooled to -70°C, treated with n-BuLi in hexane, stirred for 10 min, mixt. was added to slurryof CO2 in THF, mixt. was allowed to warm to room temp., hydrolyzed, adjusted to pH 5 by CH3COOH; THF was removed by rotary evaporator, solid was suspended in aq. phase,filtered, washed with H2O, dried in vac. at room temp., EtOH soln. of KOH was added, recrystd. from EtOH; elem. anal.;
DOI:10.1021/ja00370a016