oxalomonohydroximic acid-2-amid-1-anilide

Base Information

• Chemical Name: oxalomonohydroximic acid-2-amid-1-anilide
• CAS No.: 92875-90-6
• Molecular Formula: C₈H₉N₃O₂
• Molecular Weight: 179.178
• Mol file: 92875-90-6.mol

Synonyms:

Chemical Property of oxalomonohydroximic acid-2-amid-1-anilide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of oxalomonohydroximic acid-2-amid-1-anilide

There total 5 articles about oxalomonohydroximic acid-2-amid-1-anilide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-phenylcyanoformamidoxime (90004-03-8) → oxalomonohydroximic acid-2-amid-1-anilide (92875-90-6)

Guidance literature:

With hydrogen bromide; In acetic acid;

DOI:10.1002/hlca.19640470107

Reference yield:

N-nitroso-N-phenyl-glycine nitrile (827-51-0) → oxalomonohydroximic acid-2-amid-1-anilide (92875-90-6)

Guidance literature:

Multi-step reaction with 2 steps

1: NaOMe / methanol

2: aq. HBr / acetic acid

With hydrogen bromide; sodium methylate; In methanol; acetic acid;

DOI:10.1002/hlca.19640470107

Reference yield:

aniline (62-53-3) → oxalomonohydroximic acid-2-amid-1-anilide (92875-90-6)

Guidance literature:

Multi-step reaction with 2 steps

2: diethyl ether; water; ammonia

With diethyl ether; ammonia; water;

upstream raw materials:

ethyl 2-anilino-2-(hydroxyimino)acetate

chlorooximidoacetamide

aniline

N-phenylcyanoformamidoxime

Downstream raw materials:

phenyl-oxalamide