carbonic acid 1-{N-benzyl-N'-[(2,6-dimethyl-phenoxy)-acetyl]-hydrazinocarbonyl}-2-(2-tert-butoxycarbonylamino-3-methylsulfanyl-propionylamino)-3-phenyl-propyl ester isobutyl ester

Base Information

Chemical Name:carbonic acid 1-{N-benzyl-N'-[(2,6-dimethyl-phenoxy)-acetyl]-hydrazinocarbonyl}-2-(2-tert-butoxycarbonylamino-3-methylsulfanyl-propionylamino)-3-phenyl-propyl ester isobutyl ester
CAS No.:521275-30-9
Molecular Formula:C₄₁H₅₄N₄O₉S
Molecular Weight:778.967
Hs Code.:

carbonic acid 1-{<i>N</i>-benzyl-<i>N</i>'-[(2,6-dimethyl-phenoxy)-acetyl]-hydrazinocarbonyl}-2-(2-<i>tert</i>-butoxycarbonylamino-3-methylsulfanyl-propionylamino)-3-phenyl-propyl ester isobutyl ester

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Chemical Property of carbonic acid 1-{N-benzyl-N'-[(2,6-dimethyl-phenoxy)-acetyl]-hydrazinocarbonyl}-2-(2-tert-butoxycarbonylamino-3-methylsulfanyl-propionylamino)-3-phenyl-propyl ester isobutyl ester

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Technology Process of carbonic acid 1-{N-benzyl-N'-[(2,6-dimethyl-phenoxy)-acetyl]-hydrazinocarbonyl}-2-(2-tert-butoxycarbonylamino-3-methylsulfanyl-propionylamino)-3-phenyl-propyl ester isobutyl ester

There total 5 articles about carbonic acid 1-{N-benzyl-N'-[(2,6-dimethyl-phenoxy)-acetyl]-hydrazinocarbonyl}-2-(2-tert-butoxycarbonylamino-3-methylsulfanyl-propionylamino)-3-phenyl-propyl ester isobutyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13335-71-2
2-(2,6-dimethylphenoxy)acetic acid

: 521275-30-9
carbonic acid 1-{N-benzyl-N'-[(2,6-dimethyl-phenoxy)-acetyl]-hydrazinocarbonyl}-2-(2-tert-butoxycarbonylamino-3-methylsulfanyl-propionylamino)-3-phenyl-propyl ester isobutyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: Et₃N; BOP / dimethylformamide

2: NMM / dimethylformamide

3: HCl / dioxane

4: Et₃N; BOP / dimethylformamide

With 4-methyl-morpholine; hydrogenchloride; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(02)00848-X

Reference yield:

: 555-96-4
Benzylhydrazine

: 521275-30-9
carbonic acid 1-{N-benzyl-N'-[(2,6-dimethyl-phenoxy)-acetyl]-hydrazinocarbonyl}-2-(2-tert-butoxycarbonylamino-3-methylsulfanyl-propionylamino)-3-phenyl-propyl ester isobutyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: Et₃N; BOP / dimethylformamide

2: NMM / dimethylformamide

3: HCl / dioxane

4: Et₃N; BOP / dimethylformamide

With 4-methyl-morpholine; hydrogenchloride; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(02)00848-X

Reference yield:

: 521275-19-4
(2,6-dimethyl-phenoxy)-acetic acid N'-benzyl-hydrazide

: 521275-30-9
carbonic acid 1-{N-benzyl-N'-[(2,6-dimethyl-phenoxy)-acetyl]-hydrazinocarbonyl}-2-(2-tert-butoxycarbonylamino-3-methylsulfanyl-propionylamino)-3-phenyl-propyl ester isobutyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: NMM / dimethylformamide

2: HCl / dioxane

3: Et₃N; BOP / dimethylformamide

With 4-methyl-morpholine; hydrogenchloride; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(02)00848-X