tetrabutylammonium benzyladipate

Base Information

• Chemical Name: tetrabutylammonium benzyladipate
• CAS No.: 87353-23-9
• Molecular Formula: C₁₃H₁₅O₄*C₁₆H₃₆N
• Molecular Weight: 477.728
• Mol file: 87353-23-9.mol

Synonyms:

Chemical Property of tetrabutylammonium benzyladipate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of tetrabutylammonium benzyladipate

There total 4 articles about tetrabutylammonium benzyladipate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Adipic acid (124-04-9) → tetrabutylammonium benzyladipate (87353-23-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 40 percent / p-toluenesulfonic acid / toluene / Heating

2: 1.) NaHCO₃ / 2.) CHCl₃, 5 min

With sodium hydrogencarbonate; toluene-4-sulfonic acid; In toluene;

DOI:10.1021/jm00163a055

Reference yield:

benzyl alcohol (100-51-6,185532-71-2) → tetrabutylammonium benzyladipate (87353-23-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 40 percent / p-toluenesulfonic acid / toluene / Heating

2: 1.) NaHCO₃ / 2.) CHCl₃, 5 min

With sodium hydrogencarbonate; toluene-4-sulfonic acid; In toluene;

DOI:10.1021/jm00163a055

Reference yield:

adipic acid monobenzyl ester (40542-90-3) + tetra(n-butyl)ammonium hydrogensulfate (32503-27-8) → tetrabutylammonium benzyladipate (87353-23-9)

Guidance literature:

With sodium hydrogencarbonate; Yield given. Multistep reaction; 2.) CHCl₃, 5 min;

DOI:10.1021/jm00163a055

upstream raw materials:

adipic acid monobenzyl ester

tetra(n-butyl)ammonium hydrogensulfate

Adipic acid

benzyl alcohol

Downstream raw materials:

{[6-(benzyloxy)adipoyl]oxy}methyl penicillanate sulfone

Refernces

• 1、 -. "1,1-Alkanediol dicarboxylate linked antibacterial agents". . . Retrieved 2008/06/13.