(N,N'-para-methoxyphenyl-diazabutadiene)tetracarbonyl molybdenum complex

Base Information

Chemical Name:(N,N'-para-methoxyphenyl-diazabutadiene)tetracarbonyl molybdenum complex
CAS No.:31021-61-1
Molecular Formula:C₂₀H₁₆MoN₂O₆
Molecular Weight:476.297
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Technology Process of (N,N'-para-methoxyphenyl-diazabutadiene)tetracarbonyl molybdenum complex

There total 1 articles about (N,N'-para-methoxyphenyl-diazabutadiene)tetracarbonyl molybdenum complex which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 24978-42-5,24764-91-8
1,4-bis(4'-methoxyphenyl)-1,4-diazabuta-1,3-diene

: 13939-06-5,199620-15-0
molybdenum hexacarbonyl

: 31021-61-1
(N,N'-para-methoxyphenyl-diazabutadiene)tetracarbonyl molybdenum complex

Guidance literature:: With tetrahydrofuran; In tetrahydrofuran; Irradiation (UV/VIS); std. Schlenk techniques and vac.-line manipulatuions; soln. of 1.5 moleequiv. of Mo(CO)6 photolyzed with 150 W high pressure mercury lamp for 2 h; soln. of p-methoxyphenyl-diazabutadiene added; stirred for 48 h at ambient temp.; solvent and volatile materials removed in vac.; residue chromd. (Al2O3,ether/n-hexane); sublimation at reduced pressure; elem. anal.;
DOI:10.1016/S0020-1693(99)00418-1