{(S)-5-[(S)-1-[(R)-1-({[(S)-1-Benzyl-2-(N'-butyryl-hydrazino)-2-oxo-ethylcarbamoyl]-methyl}-carbamoyl)-ethylcarbamoyl]-2-(4-hydroxy-phenyl)-ethylcarbamoyl]-5-benzyloxycarbonylamino-pentyl}-carbamic acid benzyl ester

Base Information

• Chemical Name: {(S)-5-[(S)-1-[(R)-1-({[(S)-1-Benzyl-2-(N'-butyryl-hydrazino)-2-oxo-ethylcarbamoyl]-methyl}-carbamoyl)-ethylcarbamoyl]-2-(4-hydroxy-phenyl)-ethylcarbamoyl]-5-benzyloxycarbonylamino-pentyl}-carbamic acid benzyl ester
• CAS No.: 81378-85-0
• Molecular Formula: C₄₉H₆₀N₈O₁₁
• Molecular Weight: 937.062

Synonyms:

Chemical Property of {(S)-5-[(S)-1-[(R)-1-({[(S)-1-Benzyl-2-(N'-butyryl-hydrazino)-2-oxo-ethylcarbamoyl]-methyl}-carbamoyl)-ethylcarbamoyl]-2-(4-hydroxy-phenyl)-ethylcarbamoyl]-5-benzyloxycarbonylamino-pentyl}-carbamic acid benzyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of {(S)-5-[(S)-1-[(R)-1-({[(S)-1-Benzyl-2-(N'-butyryl-hydrazino)-2-oxo-ethylcarbamoyl]-methyl}-carbamoyl)-ethylcarbamoyl]-2-(4-hydroxy-phenyl)-ethylcarbamoyl]-5-benzyloxycarbonylamino-pentyl}-carbamic acid benzyl ester

There total 1 articles about {(S)-5-[(S)-1-[(R)-1-({[(S)-1-Benzyl-2-(N'-butyryl-hydrazino)-2-oxo-ethylcarbamoyl]-methyl}-carbamoyl)-ethylcarbamoyl]-2-(4-hydroxy-phenyl)-ethylcarbamoyl]-5-benzyloxycarbonylamino-pentyl}-carbamic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(S)-2,6-Bis-benzyloxycarbonylamino-hexanoic acid 3,5-dioxo-4-aza-tricyclo[5.2.1.02,6]dec-8-en-4-yl ester (97975-65-0) + (S)-2-Amino-N-[(R)-1-({[(S)-1-benzyl-2-(N'-butyryl-hydrazino)-2-oxo-ethylcarbamoyl]-methyl}-carbamoyl)-ethyl]-3-(4-hydroxy-phenyl)-propionamide (72732-45-7) → {(S)-5-[(S)-1-[(R)-1-({[(S)-1-Benzyl-2-(N'-butyryl-hydrazino)-2-oxo-ethylcarbamoyl]-methyl}-carbamoyl)-ethylcarbamoyl]-2-(4-hydroxy-phenyl)-ethylcarbamoyl]-5-benzyloxycarbonylamino-pentyl}-carbamic acid benzyl ester (81378-85-0)

Guidance literature:

With TEA; In N,N-dimethyl-formamide; Ambient temperature;

DOI:10.1248/cpb.29.3639

Reference yield:

{(S)-5-[(S)-1-[(R)-1-({[(S)-1-Benzyl-2-(N'-butyryl-hydrazino)-2-oxo-ethylcarbamoyl]-methyl}-carbamoyl)-ethylcarbamoyl]-2-(4-hydroxy-phenyl)-ethylcarbamoyl]-5-benzyloxycarbonylamino-pentyl}-carbamic acid benzyl ester (81378-85-0) → (S)-2,6-Diamino-hexanoic acid [(S)-1-[(R)-1-({[(S)-1-benzyl-2-(N'-butyryl-hydrazino)-2-oxo-ethylcarbamoyl]-methyl}-carbamoyl)-ethylcarbamoyl]-2-(4-hydroxy-phenyl)-ethyl]-amide (81378-90-7)

Guidance literature:

With hydrogen; palladium; In methanol;

DOI:10.1248/cpb.29.3639

upstream raw materials:

(S)-2,6-Bis-benzyloxycarbonylamino-hexanoic acid 3,5-dioxo-4-aza-tricyclo[5.2.1.0^2,6]dec-8-en-4-yl ester

(S)-2-Amino-N-[(R)-1-({[(S)-1-benzyl-2-(N'-butyryl-hydrazino)-2-oxo-ethylcarbamoyl]-methyl}-carbamoyl)-ethyl]-3-(4-hydroxy-phenyl)-propionamide

Downstream raw materials:

(S)-2,6-Diamino-hexanoic acid [(S)-1-[(R)-1-({[(S)-1-benzyl-2-(N'-butyryl-hydrazino)-2-oxo-ethylcarbamoyl]-methyl}-carbamoyl)-ethylcarbamoyl]-2-(4-hydroxy-phenyl)-ethyl]-amide

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