Technology Process of C74H84Br2O4
There total 3 articles about C74H84Br2O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrakis(triphenylphosphine) palladium(0); sodium hydrogencarbonate;
In
tetrahydrofuran; water;
for 24h;
Reflux;
DOI:10.1021/ma9024448
- Guidance literature:
-
Multi-step reaction with 3 steps
1: thionyl chloride / 10 h / Reflux
2: aluminum (III) chloride / dichloromethane / 2 h / 20 °C
3: tetrakis(triphenylphosphine) palladium(0); sodium hydrogencarbonate / tetrahydrofuran; water / 24 h / Reflux
With
aluminum (III) chloride; tetrakis(triphenylphosphine) palladium(0); thionyl chloride; sodium hydrogencarbonate;
In
tetrahydrofuran; dichloromethane; water;
2: Friedel Crafts alkylation / 3: Suzuki coupling;
DOI:10.1021/ma9024448
- Guidance literature:
-
Multi-step reaction with 2 steps
1: aluminum (III) chloride / dichloromethane / 2 h / 20 °C
2: tetrakis(triphenylphosphine) palladium(0); sodium hydrogencarbonate / tetrahydrofuran; water / 24 h / Reflux
With
aluminum (III) chloride; tetrakis(triphenylphosphine) palladium(0); sodium hydrogencarbonate;
In
tetrahydrofuran; dichloromethane; water;
1: Friedel Crafts alkylation / 2: Suzuki coupling;
DOI:10.1021/ma9024448
