C₃₈H₅₀O₉

Base Information

Chemical Name:C₃₈H₅₀O₉
CAS No.:141276-86-0
Molecular Formula:C₃₈H₅₀O₉
Molecular Weight:650.81
Hs Code.:

C<sub>38</sub>H<sub>50</sub>O<sub>9</sub>

Synonyms:

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Chemical Property of C₃₈H₅₀O₉

Chemical Property:

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Technology Process of C₃₈H₅₀O₉

There total 17 articles about C₃₈H₅₀O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (1R,2S,4R,6S)-2-Hydroxymethyl-6-methoxymethoxy-cyclohexane-1,4-diol

: 141276-86-0
C₃₈H₅₀O₉

Guidance literature:: Multi-step reaction with 17 steps

1: dimethylformamide

2: NaH / dimethylformamide / Ambient temperature

3: AcOH, H₂O / Ambient temperature

4: pyridine

5: 97 percent / pyridine / 60 °C

6: 87 percent / MeONa / methanol / Ambient temperature

7: pyridinium chlorochromate (PCC) / CH₂Cl₂

8: 68 percent / potassium hexamethyldisilazane, 18-crown-6 / tetrahydrofuran / -78 °C

9: (i-Bu)2AlH / CH₂Cl₂ / -78 °C

10: 97 percent / 4-(N,N-dimethylamino)pyridine, Et₃N / CH₂Cl₂ / Ambient temperature

11: 44 percent / OsO₄, N-methylmorpholine N-oxide (NMO) / acetone; H₂O / Ambient temperature

12: 100 percent / N,N-(i-Pr)2EtN / CH₂Cl₂ / Heating

13: H₂ / 10percent Pd/C / ethanol

14: pyridinium chlorochromate (PCC) / CH₂Cl₂

15: tetrahydrofuran / Ambient temperature

16: n-Bu₄NF / tetrahydrofuran / 0 °C

17: dimethylformamide / Ambient temperature

With pyridine; dmap; osmium(VIII) oxide; potassium hexamethyldisilazane; 18-crown-6 ether; tetrabutyl ammonium fluoride; water; hydrogen; sodium methylate; sodium hydride; diisobutylaluminium hydride; acetic acid; 4-methylmorpholine N-oxide; triethylamine; N-ethyl-N,N-diisopropylamine; pyridinium chlorochromate; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetone;
DOI:10.1039/c39920000406

Reference yield:

: (4aS,6R,8S,8aR)-8-Methoxymethoxy-2,2-dimethyl-hexahydro-benzo[1,3]dioxin-6-ol

: 141276-86-0
C₃₈H₅₀O₉

Guidance literature:: Multi-step reaction with 16 steps

1: NaH / dimethylformamide / Ambient temperature

2: AcOH, H₂O / Ambient temperature

3: pyridine

4: 97 percent / pyridine / 60 °C

5: 87 percent / MeONa / methanol / Ambient temperature

6: pyridinium chlorochromate (PCC) / CH₂Cl₂

7: 68 percent / potassium hexamethyldisilazane, 18-crown-6 / tetrahydrofuran / -78 °C

8: (i-Bu)2AlH / CH₂Cl₂ / -78 °C

9: 97 percent / 4-(N,N-dimethylamino)pyridine, Et₃N / CH₂Cl₂ / Ambient temperature

10: 44 percent / OsO₄, N-methylmorpholine N-oxide (NMO) / acetone; H₂O / Ambient temperature

11: 100 percent / N,N-(i-Pr)2EtN / CH₂Cl₂ / Heating

12: H₂ / 10percent Pd/C / ethanol

13: pyridinium chlorochromate (PCC) / CH₂Cl₂

14: tetrahydrofuran / Ambient temperature

15: n-Bu₄NF / tetrahydrofuran / 0 °C

16: dimethylformamide / Ambient temperature

With pyridine; dmap; osmium(VIII) oxide; potassium hexamethyldisilazane; 18-crown-6 ether; tetrabutyl ammonium fluoride; water; hydrogen; sodium methylate; sodium hydride; diisobutylaluminium hydride; acetic acid; 4-methylmorpholine N-oxide; triethylamine; N-ethyl-N,N-diisopropylamine; pyridinium chlorochromate; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetone;
DOI:10.1039/c39920000406

Reference yield:

: (1R,2S,4R,6S)-4-Benzyloxy-2-hydroxymethyl-6-methoxymethoxy-cyclohexanol

: 141276-86-0
C₃₈H₅₀O₉

Guidance literature:: Multi-step reaction with 14 steps

1: pyridine

2: 97 percent / pyridine / 60 °C

3: 87 percent / MeONa / methanol / Ambient temperature

4: pyridinium chlorochromate (PCC) / CH₂Cl₂

5: 68 percent / potassium hexamethyldisilazane, 18-crown-6 / tetrahydrofuran / -78 °C

6: (i-Bu)2AlH / CH₂Cl₂ / -78 °C

7: 97 percent / 4-(N,N-dimethylamino)pyridine, Et₃N / CH₂Cl₂ / Ambient temperature

8: 44 percent / OsO₄, N-methylmorpholine N-oxide (NMO) / acetone; H₂O / Ambient temperature

9: 100 percent / N,N-(i-Pr)2EtN / CH₂Cl₂ / Heating

10: H₂ / 10percent Pd/C / ethanol

11: pyridinium chlorochromate (PCC) / CH₂Cl₂

12: tetrahydrofuran / Ambient temperature

13: n-Bu₄NF / tetrahydrofuran / 0 °C

14: dimethylformamide / Ambient temperature

With pyridine; dmap; osmium(VIII) oxide; potassium hexamethyldisilazane; 18-crown-6 ether; tetrabutyl ammonium fluoride; hydrogen; sodium methylate; diisobutylaluminium hydride; 4-methylmorpholine N-oxide; triethylamine; N-ethyl-N,N-diisopropylamine; pyridinium chlorochromate; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetone;
DOI:10.1039/c39920000406