(R)-3-Hydroxymethyl-2,2,3-trimethyl-5-[1-phenyl-meth-(Z)-ylidene]-cyclopentanol

Base Information

Chemical Name:(R)-3-Hydroxymethyl-2,2,3-trimethyl-5-[1-phenyl-meth-(Z)-ylidene]-cyclopentanol
CAS No.:87798-62-7
Molecular Formula:C₁₆H₂₂O₂
Molecular Weight:246.349
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-3-Hydroxymethyl-2,2,3-trimethyl-5-[1-phenyl-meth-(Z)-ylidene]-cyclopentanol

Chemical Property:

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Technology Process of (R)-3-Hydroxymethyl-2,2,3-trimethyl-5-[1-phenyl-meth-(Z)-ylidene]-cyclopentanol

There total 8 articles about (R)-3-Hydroxymethyl-2,2,3-trimethyl-5-[1-phenyl-meth-(Z)-ylidene]-cyclopentanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 87798-68-3
5-benzylidene-3-hydroxymethyl-2,2,3-trimethylcyclopentan-1-one

: 87798-62-7,87859-85-6
(R)-3-Hydroxymethyl-2,2,3-trimethyl-5-[1-phenyl-meth-(Z)-ylidene]-cyclopentanol

Guidance literature:: With sodium hydroxide; sodium tetrahydroborate; In methanol; at 20 ℃; for 24h;

Reference yield:

: 124-83-4
D-(+)-camphoric acid

: 87798-62-7,87859-85-6
(R)-3-Hydroxymethyl-2,2,3-trimethyl-5-[1-phenyl-meth-(Z)-ylidene]-cyclopentanol

Guidance literature:: Multi-step reaction with 8 steps

1: 83 percent / phosphorus pentachloride

2: 85 percent / ice, water / dimethylformamide

3: 87 percent / 0.1N-sulphuric acid / Heating

4: 91 percent / sulphuric acid

5: 90 percent / lithium aluminium hydride / diethyl ether / 18 h / Heating

6: periodic acid / H₂O / 1 h / 20 °C

7: 82 percent / potassium hydroxide / ethanol; H₂O / 1.) reflux, 30 min, 2.) 20 deg C, 18 h

8: 95 percent / sodium borohydride, sodium hydroxide / methanol / 24 h / 20 °C

With potassium hydroxide; sodium hydroxide; sodium tetrahydroborate; lithium aluminium tetrahydride; phosphorus pentachloride; sulfuric acid; Methamphetamin; water; periodic acid; In methanol; diethyl ether; ethanol; water; N,N-dimethyl-formamide;

Reference yield:

: 67111-66-4,13429-83-9
(-)-camphanic acid

: 87798-62-7,87859-85-6
(R)-3-Hydroxymethyl-2,2,3-trimethyl-5-[1-phenyl-meth-(Z)-ylidene]-cyclopentanol

Guidance literature:: Multi-step reaction with 5 steps

1: 91 percent / sulphuric acid

2: 90 percent / lithium aluminium hydride / diethyl ether / 18 h / Heating

3: periodic acid / H₂O / 1 h / 20 °C

4: 82 percent / potassium hydroxide / ethanol; H₂O / 1.) reflux, 30 min, 2.) 20 deg C, 18 h

5: 95 percent / sodium borohydride, sodium hydroxide / methanol / 24 h / 20 °C

With potassium hydroxide; sodium hydroxide; sodium tetrahydroborate; lithium aluminium tetrahydride; sulfuric acid; periodic acid; In methanol; diethyl ether; ethanol; water;