[C₇H₈(P₃C(1-adamantyl))(W(CO)5)2]

Base Information

• Chemical Name: [C₇H₈(P₃C(1-adamantyl))(W(CO)5)2]
• CAS No.: 1138340-23-4
• Molecular Formula: C₂₈H₂₃O₁₀P₃W₂
• Molecular Weight: 980.106

Synonyms:

Chemical Property of [C₇H₈(P₃C(1-adamantyl))(W(CO)5)2]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [C₇H₈(P₃C(1-adamantyl))(W(CO)5)2]

There total 1 articles about [C₇H₈(P₃C(1-adamantyl))(W(CO)5)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

[(W(CO)5)2P3(C(1-adamantyl)O)Nb(N(CH2(tert-butyl))(3,5-(methyl)2C6H3))3] + spiro[2.4]hepta-4,6-diene (765-46-8) → [ONb(N(CH2(tert-butyl))(3,5-(methyl)2C6H3))3] + [C7H8(P3C(1-adamantyl))(W(CO)5)2] (1138340-23-4)

Guidance literature:

In tetrahydrofuran; under anhydrous and oxygen-free conditions; W-Nb compd. dissolved in soln. of spiroheptadiene, stirred at 22°C for 5 h, filtered through celite, filtrate concd. to dryness under dynamic vac.; residue suspended in n-pentane (extn. of Nb compd.), cooled to -35°C for 24 h, powder collected atop sintered glass frit, washed with cold pentane;

DOI:10.1002/anie.200804432

upstream raw materials:

spiro[2.4]hepta-4,6-diene

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 1138340-23-4 [C₇H₈(P₃C(1-adamantyl))(W(CO)5)2]

Send

Send

Metric Ton KG G Pound L ML

Send

Send