C₅₂H₄₇N₃O₁₆

Base Information

Chemical Name:C₅₂H₄₇N₃O₁₆
CAS No.:1589028-55-6
Molecular Formula:C₅₂H₄₇N₃O₁₆
Molecular Weight:969.956
Hs Code.:

C<sub>52</sub>H<sub>47</sub>N<sub>3</sub>O<sub>16</sub>

Synonyms:

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Chemical Property of C₅₂H₄₇N₃O₁₆

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Technology Process of C₅₂H₄₇N₃O₁₆

There total 8 articles about C₅₂H₄₇N₃O₁₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: C₄₆H₄₃ClN₂O₁₃

: 1589028-55-6
C₅₂H₄₇N₃O₁₆

Guidance literature:: With triethylamine; In dichloromethane;
DOI:10.1039/c3ra47633b

Reference yield:

: 54845-07-7
2-(3,5-dihydroxyphenyl)isoindoline-1,3-dione

: 1589028-55-6
C₅₂H₄₇N₃O₁₆

Guidance literature:: Multi-step reaction with 7 steps

1: potassium carbonate / N,N-dimethyl-formamide / 90 °C

2: hydrazine hydrate / ethanol / Reflux

3: dmap; 1H-imidazole / 130 °C

4: toluene-4-sulfonic acid / toluene / 95 °C

5: 1H-imidazole / N,N-dimethyl-formamide / 95 °C

6: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 2 h / 20 °C

7: triethylamine / dichloromethane

With 1H-imidazole; dmap; oxalyl dichloride; potassium carbonate; toluene-4-sulfonic acid; hydrazine hydrate; triethylamine; N,N-dimethyl-formamide; In ethanol; dichloromethane; N,N-dimethyl-formamide; toluene; 2: |Gabriel Amine Synthesis;
DOI:10.1039/c3ra47633b

Reference yield:

: 1589028-28-3
C₂₈H₃₇NO₁₀

: 1589028-55-6
C₅₂H₄₇N₃O₁₆

Guidance literature:: Multi-step reaction with 6 steps

1: hydrazine hydrate / ethanol / Reflux

2: dmap; 1H-imidazole / 130 °C

3: toluene-4-sulfonic acid / toluene / 95 °C

4: 1H-imidazole / N,N-dimethyl-formamide / 95 °C

5: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 2 h / 20 °C

6: triethylamine / dichloromethane

With 1H-imidazole; dmap; oxalyl dichloride; toluene-4-sulfonic acid; hydrazine hydrate; triethylamine; N,N-dimethyl-formamide; In ethanol; dichloromethane; N,N-dimethyl-formamide; toluene; 1: |Gabriel Amine Synthesis;
DOI:10.1039/c3ra47633b