8-oxo-5,6-dihydro-4H,8H-[1,2,5]oxadiazolo[3,4-c]pyrido[3,2,1-ij]quinolin-9-ium-9-olate

Base Information

Chemical Name:8-oxo-5,6-dihydro-4H,8H-[1,2,5]oxadiazolo[3,4-c]pyrido[3,2,1-ij]quinolin-9-ium-9-olate
CAS No.:141945-44-0
Molecular Formula:C₁₂H₉N₃O₃
Molecular Weight:243.222
Hs Code.:
DSSTox Substance ID:DTXSID20380735

Synonyms:8-oxo-5,6-dihydro-4H,8H-[1,2,5]oxadiazolo[3,4-c]pyrido[3,2,1-ij]quinolin-9-ium-9-olate;141945-44-0;13-oxido-12-oxa-1,11-diaza-13-azoniatetracyclo[7.6.1.05,16.010,14]hexadeca-5(16),6,8,10,13-pentaen-15-one;DTXSID20380735

Suppliers and Price of 8-oxo-5,6-dihydro-4H,8H-[1,2,5]oxadiazolo[3,4-c]pyrido[3,2,1-ij]quinolin-9-ium-9-olate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 8-oxo-5,6-dihydro-4H,8H-[1,2,5]oxadiazolo[3,4-c]pyrido[3,2,1-ij]quinolin-9-ium-9-olate

Chemical Property:

Vapor Pressure:6.37E-11mmHg at 25°C
XLogP3:1.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:0
Exact Mass:243.06439116
Heavy Atom Count:18
Complexity:378

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1CC2=C3C(=CC=C2)C4=NO[N+](=C4C(=O)N3C1)[O-]

Technology Process of 8-oxo-5,6-dihydro-4H,8H-[1,2,5]oxadiazolo[3,4-c]pyrido[3,2,1-ij]quinolin-9-ium-9-olate

There total 7 articles about 8-oxo-5,6-dihydro-4H,8H-[1,2,5]oxadiazolo[3,4-c]pyrido[3,2,1-ij]quinolin-9-ium-9-olate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 110216-66-5
1-azido-2-nitro-3-oxo-6,7-dihydro-3H,5H-benzoquinolizine

: 141945-44-0
8-oxo-5,6-dihydro-4H,8H-benzo-1,2,5-oxadiazolo<3,4-b>quinolizine 9-oxide

Guidance literature:: In various solvent(s); for 0.333333h; Heating;

Reference yield:

: 95594-15-3
9-hydroxy-8,11-dioxo-5,6,8,11-tetrahydro-4H-benzopyrano<2,3-b>quinolizine

: 141945-44-0
8-oxo-5,6-dihydro-4H,8H-benzo-1,2,5-oxadiazolo<3,4-b>quinolizine 9-oxide

Guidance literature:: Multi-step reaction with 6 steps

1: 99 percent / NaOH / ethane-1,2-diol; H₂O / 1 h / Heating

2: 96 percent / 90percent aq. H₂SO₄ / 15 h / 140 °C

3: 89 percent / conc. HNO₃, NaNO₂ / acetic acid / 0.5 h

4: 94 percent / triethylamine, phosphoryl chloride / 1 h / Heating

5: 89 percent / NaN₃ / various solvent(s) / 3 h / Ambient temperature

6: 92 percent / various solvent(s) / 0.33 h / Heating

With sodium hydroxide; sodium azide; sulfuric acid; nitric acid; triethylamine; sodium nitrite; trichlorophosphate; In water; ethylene glycol; acetic acid;

Reference yield:

: 635-46-1
1,2,3,4-tetrahydroisoquinoline

: 141945-44-0
8-oxo-5,6-dihydro-4H,8H-benzo-1,2,5-oxadiazolo<3,4-b>quinolizine 9-oxide

Guidance literature:: Multi-step reaction with 7 steps

1: 60 percent / diphenyl ether / 5 h / Heating

2: 99 percent / NaOH / ethane-1,2-diol; H₂O / 1 h / Heating

3: 96 percent / 90percent aq. H₂SO₄ / 15 h / 140 °C

4: 89 percent / conc. HNO₃, NaNO₂ / acetic acid / 0.5 h

5: 94 percent / triethylamine, phosphoryl chloride / 1 h / Heating

6: 89 percent / NaN₃ / various solvent(s) / 3 h / Ambient temperature

7: 92 percent / various solvent(s) / 0.33 h / Heating

With sodium hydroxide; sodium azide; sulfuric acid; nitric acid; triethylamine; sodium nitrite; trichlorophosphate; In diphenylether; water; ethylene glycol; acetic acid;