(R,S)-2-(N,N-dimethylaminomethyl)ferrocenyl(4-fluorophenyl)dimethylsilane

Base Information

Chemical Name:(R,S)-2-(N,N-dimethylaminomethyl)ferrocenyl(4-fluorophenyl)dimethylsilane
CAS No.:468732-05-0
Molecular Formula:C₂₁H₂₆FFeNSi
Molecular Weight:395.375
Hs Code.:

Synonyms:

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Chemical Property of (R,S)-2-(N,N-dimethylaminomethyl)ferrocenyl(4-fluorophenyl)dimethylsilane

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of (R,S)-2-(N,N-dimethylaminomethyl)ferrocenyl(4-fluorophenyl)dimethylsilane

There total 1 articles about (R,S)-2-(N,N-dimethylaminomethyl)ferrocenyl(4-fluorophenyl)dimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: [α-(N,N-dimethylaminomethyl)ferrocenyl]lithium

: 2355-86-4
(4-fluorophenyl)chlorodimethylsilane

: 468732-05-0
(R,S)-2-(N,N-dimethylaminomethyl)ferrocenyl(4-fluorophenyl)dimethylsilane

Guidance literature:: In tetrahydrofuran; pentane; byproducts: LiCl; a suspn. of Li-compound and THF was added slowly to a stirred soln. of silane in n-pentane at -78°C, the mixt. was warmed to ambient temp., stirred overnight (Ar); evapd., dissolved in n-pentane, filtered, the solvent was removed under reduced pressure; as oil;
DOI:10.1016/S0022-328X(02)01427-4

Reference yield: 95.0%

: 7647-01-0,15364-23-5
hydrogenchloride

: 468732-05-0
(R,S)-2-(N,N-dimethylaminomethyl)ferrocenyl(4-fluorophenyl)dimethylsilane

: 7732-18-5
water

: (R,S)-2-(N,N-dimethylaminomethyl)ferrocenyl(4-fluorophenyl)dimethylsilane hydrogen chloride dihydrate

Guidance literature:: In pentane; a stream of gaseous HCl was flushed slowly through the soln. of complex in n-pentane at 0°C for 30 min, the mixt. was warmed to ambient temp. and stirred overnight at room temp.; ppt. was filtered, washed with a little bit of n-pentane, dried in a stream of Ar and under oil-pump vac.;elem. anal.;
DOI:10.1016/S0022-328X(02)01427-4

Reference yield:

: 468732-05-0
(R,S)-2-(N,N-dimethylaminomethyl)ferrocenyl(4-fluorophenyl)dimethylsilane

: 88-89-1
2,4,6-Trinitrophenol

: 468732-10-7
(R,S)-2-(N,N-dimethylaminomethyl)ferrocenyl(4-fluorophenyl)dimethylsilane picrate

Guidance literature:: In ethanol; an ethanolic soln. of picric acid was added dropwise to a soln. of complex in ethanol, the suspn. was warmed for 3 min (Ar); ppt. was washed with cold ethanol and diethyl ether, recrystd. from hot acetone-isopropanol; elem. anal.;
DOI:10.1016/S0022-328X(02)01427-4