W₂[bis(ethylamido)phenylborane]3

Base Information

• Chemical Name: W₂[bis(ethylamido)phenylborane]3
• CAS No.: 726137-82-2
• Molecular Formula: C₃₀H₄₅B₃N₆W₂
• Molecular Weight: 889.861

Synonyms:

Chemical Property of W₂[bis(ethylamido)phenylborane]3

Chemical Property:

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Technology Process of W₂[bis(ethylamido)phenylborane]3

There total 1 articles about W₂[bis(ethylamido)phenylborane]3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.8%

NaW2Cl7(THF)5 + bis(ethylamido)phenylborane dithio salt*(diethyl ether) → W2[bis(ethylamido)phenylborane]3 (726137-82-2)

Guidance literature:

In tetrahydrofuran; byproducts: LiCl; under N2; THF soln. of W complex frozen; suspn. of Li salt in THF added dropwise over 3 min; warmed slowly to room temp.; stirred overnight; solvent removed by vac. evapn.; pentane added; filtered through Celite; filtrate concd.; cooled to -35°C; crystals collected by filtration; elem. anal.;

DOI:10.1021/ic049795r

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