(E)-3-(2-iodo-6-nitrophenyl)-2-phenylpropenoic acid

Base Information

Chemical Name:(E)-3-(2-iodo-6-nitrophenyl)-2-phenylpropenoic acid
CAS No.:117847-42-4
Molecular Formula:C₁₅H₁₀INO₄
Molecular Weight:395.153
Hs Code.:

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Chemical Property of (E)-3-(2-iodo-6-nitrophenyl)-2-phenylpropenoic acid

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Technology Process of (E)-3-(2-iodo-6-nitrophenyl)-2-phenylpropenoic acid

There total 3 articles about (E)-3-(2-iodo-6-nitrophenyl)-2-phenylpropenoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 96839-34-8
2,6-dinitrobenzyl alcohol

: 117847-42-4
(E)-3-(2-iodo-6-nitrophenyl)-2-phenylpropenoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 66 percent / cyclohexene / 10percent palladium-charcoal / ethanol / 3.5 h / Heating

2: 1.) sodium nitrite, hydrochloric acid, 2.) potassium iodide / 1.) wwater, 2.) water, 2 h, room temperature then heated, 1h

3: 92 percent / manganese dioxide / benzene / 2 h

4: 49 percent / acetic anhydride, triethylamine / 5 h / Heating

With hydrogenchloride; manganese(IV) oxide; acetic anhydride; triethylamine; potassium iodide; cyclohexene; sodium nitrite; palladium on activated charcoal; In ethanol; benzene;

Reference yield:

: 117847-40-2
(2-iodo-6-nitrophenyl)methanol

: 117847-42-4
(E)-3-(2-iodo-6-nitrophenyl)-2-phenylpropenoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / manganese dioxide / benzene / 2 h

2: 49 percent / acetic anhydride, triethylamine / 5 h / Heating

With manganese(IV) oxide; acetic anhydride; triethylamine; In benzene;

Reference yield:

: 98451-51-5
2-amino-6-nitrobenzyl alcohol

: 117847-42-4
(E)-3-(2-iodo-6-nitrophenyl)-2-phenylpropenoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) sodium nitrite, hydrochloric acid, 2.) potassium iodide / 1.) wwater, 2.) water, 2 h, room temperature then heated, 1h

2: 92 percent / manganese dioxide / benzene / 2 h

3: 49 percent / acetic anhydride, triethylamine / 5 h / Heating

With hydrogenchloride; manganese(IV) oxide; acetic anhydride; triethylamine; potassium iodide; sodium nitrite; In benzene;