C₁₄H₂₁⁽²⁾HO

Base Information

• Chemical Name: C₁₄H₂₁⁽²⁾HO
• CAS No.: 139621-56-0
• Molecular Formula: C₁₄H₂₂O
• Molecular Weight: 207.32
• Mol file: 139621-56-0.mol

Synonyms:

Chemical Property of C₁₄H₂₁⁽²⁾HO

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₄H₂₁⁽²⁾HO

There total 9 articles about C₁₄H₂₁⁽²⁾HO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

6-Methyl-6-(4-methyl-4-pentenyl)-1-cyclohexenecarbonitrile (139621-35-5) → C14H21(2)HO (139621-56-0)

Guidance literature:

With diisobutylaluminium deuteride;

DOI:10.1002/recl.19921110104

Reference yield:

5-chloro-2-pentanone (5891-21-4) → C14H21(2)HO (139621-56-0)

Guidance literature:

Multi-step reaction with 7 steps

1: 1) n-BuLi / 1) THF, hexane, 0 deg C, 1 h, 2) 0 deg C, 2 h

2: 83 percent / NaI / acetone / 16 h / Heating

4: NaOH / 14 h / Heating

5: 98 percent / ZnI₂ / benzene / 5 h / Heating

6: 1) pyridine, POCl₃, 2) 1.3 N HCl / 1) benzene, reflux, 46 h

7: 77 percent / diisobutylaluminium deuteride

With pyridine; hydrogenchloride; sodium hydroxide; n-butyllithium; diisobutylaluminium deuteride; sodium iodide; zinc(II) iodide; trichlorophosphate; In acetone; benzene;

DOI:10.1002/recl.19921110104

Reference yield:

5-Chloro-2-methyl-1-pentene (22508-65-2) → C14H21(2)HO (139621-56-0)

Guidance literature:

Multi-step reaction with 6 steps

1: 83 percent / NaI / acetone / 16 h / Heating

3: NaOH / 14 h / Heating

4: 98 percent / ZnI₂ / benzene / 5 h / Heating

5: 1) pyridine, POCl₃, 2) 1.3 N HCl / 1) benzene, reflux, 46 h

6: 77 percent / diisobutylaluminium deuteride

With pyridine; hydrogenchloride; sodium hydroxide; diisobutylaluminium deuteride; sodium iodide; zinc(II) iodide; trichlorophosphate; In acetone; benzene;

DOI:10.1002/recl.19921110104

upstream raw materials:

6-Methyl-6-(4-methyl-4-pentenyl)-1-cyclohexenecarbonitrile

5-chloro-2-pentanone

5-Chloro-2-methyl-1-pentene

5-iodo-2-methylpent-1-en