Technology Process of C39H30ClN5O8
There total 7 articles about C39H30ClN5O8 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 69 percent / pyridine / benzene / 0.5 h / -35 °C
2: 77 percent / 1,5-diazabicyclo<4.3.0>non-5-ene / pyridine / 3 h / 20 °C
3: pyridine / 48 h / Ambient temperature
4: 94 percent / iodine, lead carbonate / 1 h / Ambient temperature
5: 1.) 0.2 M barium hydroxide, 2.) pyridine / 1.) methanol, 15 min., 2.) methanol, 48 h., room temp.
6: dimethylsulfoxide / 70 h / 115 - 120 °C
With
pyridine; barium dihydroxide; lead Carbonate; DBN; iodine;
In
pyridine; dimethyl sulfoxide; benzene;
DOI:10.1016/S0008-6215(00)81045-9
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1.) 0.2 M barium hydroxide, 2.) pyridine / 1.) methanol, 15 min., 2.) methanol, 48 h., room temp.
2: dimethylsulfoxide / 70 h / 115 - 120 °C
With
pyridine; barium dihydroxide;
In
dimethyl sulfoxide;
DOI:10.1016/S0008-6215(00)81045-9
- Guidance literature:
-
Multi-step reaction with 4 steps
1: pyridine / 48 h / Ambient temperature
2: 94 percent / iodine, lead carbonate / 1 h / Ambient temperature
3: 1.) 0.2 M barium hydroxide, 2.) pyridine / 1.) methanol, 15 min., 2.) methanol, 48 h., room temp.
4: dimethylsulfoxide / 70 h / 115 - 120 °C
With
pyridine; barium dihydroxide; lead Carbonate; iodine;
In
dimethyl sulfoxide;
DOI:10.1016/S0008-6215(00)81045-9
