N₂C₃H(C₆H₅)(CH₂N(CH₂C₅H₄N)CH₂C₅H₄N)2

Base Information

Chemical Name:N₂C₃H(C₆H₅)(CH₂N(CH₂C₅H₄N)CH₂C₅H₄N)2
CAS No.:1295578-65-2
Molecular Formula:C₃₅H₃₄N₈
Molecular Weight:566.709
Hs Code.:

N<sub>2</sub>C<sub>3</sub>H(C<sub>6</sub>H<sub>5</sub>)(CH<sub>2</sub>N(CH<sub>2</sub>C<sub>5</sub>H<sub>4</sub>N)CH<sub>2</sub>C<sub>5</sub>H<sub>4</sub>N)2

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Suppliers and Price of N₂C₃H(C₆H₅)(CH₂N(CH₂C₅H₄N)CH₂C₅H₄N)2

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N₂C₃H(C₆H₅)(CH₂N(CH₂C₅H₄N)CH₂C₅H₄N)2

Chemical Property:

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Technology Process of N₂C₃H(C₆H₅)(CH₂N(CH₂C₅H₄N)CH₂C₅H₄N)2

There total 2 articles about N₂C₃H(C₆H₅)(CH₂N(CH₂C₅H₄N)CH₂C₅H₄N)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₀H₄₂N₈O

: 1295578-65-2
N₂C₃H(C₆H₅)(CH₂N(CH₂C₅H₄N)CH₂C₅H₄N)2

Guidance literature:: C₄₀H₄₂N₈O; With hydrogenchloride; In diethyl ether; ethanol; for 2h;

In water; pH=12; Alkaline conditions;
DOI:10.1021/om100836j

Reference yield:

: 1028491-21-5
3,5-bis(chloromethyl)-1-(tetrahydropyranyl-2-yl)-4-phenyl-1H-pyrazole

: 1539-42-0
bis[(2-pyridyl)methyl]amine

: 1295578-65-2
N₂C₃H(C₆H₅)(CH₂N(CH₂C₅H₄N)CH₂C₅H₄N)2

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium carbonate / acetonitrile / 48 h / Reflux

2.1: hydrogenchloride / diethyl ether; ethanol / 2 h

2.2: pH 12 / Alkaline conditions

With hydrogenchloride; sodium carbonate; In diethyl ether; ethanol; acetonitrile;
DOI:10.1021/om100836j

Reference yield: 75.0%

: 1295578-65-2
N₂C₃H(C₆H₅)(CH₂N(CH₂C₅H₄N)CH₂C₅H₄N)2

: mesitylcopper*0.14(toluene)

: 80937-33-3
oxygen

: ((N₂C₃(C₆H₅)(CH₂N(CH₂C₅H₄N)CH₂C₅H₄N)2)Cu₄(C₆H₂(CH₃)3)2)2O

Guidance literature:: In toluene; byproducts: mesitylene, bimesityl; under Ar; soln. of Cu compd. in toluene treated with soln. of ligand in toluene at -78°C; stirred at room temp. overnight; concd.; filtered; toluene added; O2 (dried with P2O5) slowly bubbled; stirred for 2 h; layered with Et2O; stored at -18°C for ca. 1 wk; ppt. collected by filtration; filtrate concd.; treated with pentane; filtered; repeated;combined solid fractions washed with pentane; dried in vac. for 14 h; e lem. anal.;
DOI:10.1021/om100836j