1-phenyl-2-methyl-4-benzoyl-5-benzimidazole

Base Information

• Chemical Name: 1-phenyl-2-methyl-4-benzoyl-5-benzimidazole
• CAS No.: 107479-68-5
• Molecular Formula: C₂₉H₂₇N₃O₅
• Molecular Weight: 497.55

Synonyms:

Chemical Property of 1-phenyl-2-methyl-4-benzoyl-5-benzimidazole

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 1-phenyl-2-methyl-4-benzoyl-5-benzimidazole

There total 1 articles about 1-phenyl-2-methyl-4-benzoyl-5-benzimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

1-phenyl-2-methyl-4-benzoyl-5-aminobenzimidazole (89174-94-7) + diethyl 2-ethoxymethylenemalonate (87-13-8) → 1-phenyl-2-methyl-4-benzoyl-5-benzimidazole (107479-68-5)

Guidance literature:

at 90 - 100 ℃; for 2.5h;

DOI:10.1007/BF01145804

Reference yield: 89.0%

1-phenyl-2-methyl-4-benzoyl-5-benzimidazole (107479-68-5) → 1,4-diphenyl-2-methyl-5-ethoxycarbonylimidazo<4,5-g>quinoline (107479-69-6)

Guidance literature:

With PPA; Polyphosphoric acid (PPA); 1.) 70 deg C, 2 h, 2.) 100 deg C, 1 h;

DOI:10.1007/BF01145804

Reference yield: 50.0%

1-phenyl-2-methyl-4-benzoyl-5-benzimidazole (107479-68-5) → 1-phenyl-2-methyl-4-benzoyl-7-ethoxycarbonylimidazo<5,4-g>quinolone-8 (123959-01-3)

Guidance literature:

With PPA; Polyphosphoric acid (PPA); at 90 ℃; for 3h;

DOI:10.1007/BF01145804

upstream raw materials:

1-phenyl-2-methyl-4-benzoyl-5-aminobenzimidazole

diethyl 2-ethoxymethylenemalonate

Downstream raw materials:

1,4-diphenyl-2-methyl-5-ethoxycarbonylimidazo<4,5-g>quinoline

1-phenyl-2-methyl-4-benzoyl-7-ethoxycarbonylimidazo<5,4-g>quinolone-8

1,4-diphenyl-2-methylimidazo<4,5-f>quinolinecarboxylic-5 acid

1-phenyl-2-methyl-4-benzoyl-5-ethylimidazo<5,4-g>quinoline-7-carboxylic acid

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