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2,3,5-tribromoacetophenone

Base Information
  • Chemical Name:2,3,5-tribromoacetophenone
  • CAS No.:116772-81-7
  • Molecular Formula:C8H5Br3O
  • Molecular Weight:356.839
  • Hs Code.:
2,3,5-tribromoacetophenone

Synonyms:

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The product has achieved commercial mass production*data from LookChem market partment
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Chemical Property of 2,3,5-tribromoacetophenone
Chemical Property:
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Technology Process of 2,3,5-tribromoacetophenone

There total 2 articles about 2,3,5-tribromoacetophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With hydrogen bromide; copper(I) bromide; In acetic acid; Yield given; ice-water cooling, then 80 deg C;
Guidance literature:
Multi-step reaction with 2 steps
1: NaNO2, conc. H2SO4 / acetic acid / below 20 deg C, then 1 h, 30 deg C
2: CuBr, 36percent HBr / acetic acid / ice-water cooling, then 80 deg C
With sulfuric acid; hydrogen bromide; copper(I) bromide; sodium nitrite; In acetic acid;
Guidance literature:
With potassium permanganate; deuteriated sodium hydroxide; copper aluminum; Yield given. Multistep reaction; 1.) addition gradually, 50 deg C, 140 min;
upstream raw materials:

1-(2-amino-3,5-dibromophenyl)ethanone

Downstream raw materials:

benzoic-2,3,5-d3 acid

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