N-α-(1-carboxy-3-phenylpropyl)-N^ε-benzyloxycarbonyl-L-lysyl>glycine

Base Information

Chemical Name:N-α-(1-carboxy-3-phenylpropyl)-N^ε-benzyloxycarbonyl-L-lysyl>glycine
CAS No.:126333-38-8
Molecular Formula:C₂₆H₃₃N₃O₇
Molecular Weight:499.564
Hs Code.:

N-<N<sup>α</sup>-(1-carboxy-3-phenylpropyl)-N<sup>ε</sup>-benzyloxycarbonyl-L-lysyl>glycine

Synonyms:

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Chemical Property of N-α-(1-carboxy-3-phenylpropyl)-N^ε-benzyloxycarbonyl-L-lysyl>glycine

Chemical Property:

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Technology Process of N-α-(1-carboxy-3-phenylpropyl)-N^ε-benzyloxycarbonyl-L-lysyl>glycine

There total 4 articles about N-α-(1-carboxy-3-phenylpropyl)-N^ε-benzyloxycarbonyl-L-lysyl>glycine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2389-45-9
Boc-Lys(Z)-OH

: 126333-38-8
N-α-(1-carboxy-3-phenylpropyl)-N^ε-benzyloxycarbonyl-L-lysyl>glycine

Guidance literature:: Multi-step reaction with 4 steps

1: hydroxybenzotriazole, water-soluble carbodiimide / dimethylformamide / 1 h / 0 °C

2: 5N NaOH / H₂O; ethanol / 20 h / Ambient temperature

3: trifluoroacetic acid, anisol / 1 h / -20 °C

4: 1.) molecular sieves 3A, Et₃N, 2.) NaBH₃CN, 3.) Dowex 50W-X₂ / 1.) MeOH, room temperature, 30 min, 2.) MeOH, room temperature

With sodium hydroxide; 3 A molecular sieve; DOWEX 50W-X₂; sodium cyanoborohydride; benzotriazol-1-ol; methoxybenzene; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; trifluoroacetic acid; In ethanol; water; N,N-dimethyl-formamide;

Reference yield:

: 33043-26-4
N-(N^α-tert-butoxycarbonyl-N^ε-carbobenzoxy-L-lysyl)glycine ethyl ester

: 126333-38-8
N-α-(1-carboxy-3-phenylpropyl)-N^ε-benzyloxycarbonyl-L-lysyl>glycine

Guidance literature:: Multi-step reaction with 3 steps

1: 5N NaOH / H₂O; ethanol / 20 h / Ambient temperature

2: trifluoroacetic acid, anisol / 1 h / -20 °C

3: 1.) molecular sieves 3A, Et₃N, 2.) NaBH₃CN, 3.) Dowex 50W-X₂ / 1.) MeOH, room temperature, 30 min, 2.) MeOH, room temperature

With sodium hydroxide; 3 A molecular sieve; DOWEX 50W-X₂; sodium cyanoborohydride; methoxybenzene; triethylamine; trifluoroacetic acid; In ethanol; water;

Reference yield:

: 53613-24-4
N-(N^α-tert-butoxycarbonyl-N^ε-carbobenzoxy-L-lysyl)glycine

: 126333-38-8
N-α-(1-carboxy-3-phenylpropyl)-N^ε-benzyloxycarbonyl-L-lysyl>glycine

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid, anisol / 1 h / -20 °C

2: 1.) molecular sieves 3A, Et₃N, 2.) NaBH₃CN, 3.) Dowex 50W-X₂ / 1.) MeOH, room temperature, 30 min, 2.) MeOH, room temperature

With 3 A molecular sieve; DOWEX 50W-X₂; sodium cyanoborohydride; methoxybenzene; triethylamine; trifluoroacetic acid;